Methylaminoazobenzene

Base Information

Chemical Name:Methylaminoazobenzene
CAS No.:74936-84-8
Molecular Formula:C13H13N3
Molecular Weight:211.266
Hs Code.:
DSSTox Substance ID:DTXSID901273908
Nikkaji Number:J2.252.004K

Synonyms:Methylaminoazobenzene;55914-87-9;Benzenamine, N-methyl-ar-(phenylazo)-;Monomethylaminoazobenzol;2-(Methylamino)azobenzene;74936-84-8;SCHEMBL20658883;DTXSID901273908;N-Methyl-2-(2-phenyldiazenyl)benzenamine

Suppliers and Price of Methylaminoazobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of Methylaminoazobenzene

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:211.110947427
Heavy Atom Count:16
Complexity:221

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC1=CC=CC=C1N=NC2=CC=CC=C2

Technology Process of Methylaminoazobenzene

There total 8 articles about Methylaminoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1-methyl-3-phenylaminobenzimidazolium iodide

: 74936-84-8
2-Phenyl-azo-N-methylanilin

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 5h;
DOI:10.1021/tx0000724

Reference yield:

: 88-74-4
2-nitro-aniline

: 74936-84-8
2-Phenyl-azo-N-methylanilin

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / pyridine / 15 h / 25 °C

2: 80 percent / H₂ / 5 percent Pd/C / methanol / 15 h

3: 68 percent / AcOH / ethanol / 15 h / 25 °C

4: 84 percent / KOH / methanol / 6 h / Heating

5: 42 percent / AcOH; aq. HCl / 80 °C

6: 43 percent / methanol / 96 h / 25 °C

7: 47 percent / aq. NaOH / methanol / 5 h / 20 °C

With pyridine; hydrogenchloride; potassium hydroxide; sodium hydroxide; hydrogen; acetic acid; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/tx0000724

Reference yield:

: 728-90-5
N-(2-nitrophenyl)benzanilide

: 74936-84-8
2-Phenyl-azo-N-methylanilin

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / H₂ / 5 percent Pd/C / methanol / 15 h

2: 68 percent / AcOH / ethanol / 15 h / 25 °C

3: 84 percent / KOH / methanol / 6 h / Heating

4: 42 percent / AcOH; aq. HCl / 80 °C

5: 43 percent / methanol / 96 h / 25 °C

6: 47 percent / aq. NaOH / methanol / 5 h / 20 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; hydrogen; acetic acid; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/tx0000724