2- benzoylaminoazobenzene

Base Information

• Chemical Name: 2- benzoylaminoazobenzene
• CAS No.: 7310-83-0
• Molecular Formula: C₁₉H₁₅N₃O
• Molecular Weight: 301.348
• Mol file: 7310-83-0.mol

Synonyms:2- benzoylaminoazobenzene

Chemical Property of 2- benzoylaminoazobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2- benzoylaminoazobenzene

There total 10 articles about 2- benzoylaminoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

benzamide (55-21-0,27208-38-4) + Azobenzene (1227476-15-4) → 2- benzoylaminoazobenzene (7310-83-0)

Guidance literature:

With copper diacetate; In 5,5-dimethyl-1,3-cyclohexadiene; benzene; at 120 ℃; for 24h; Reagent/catalyst; Solvent;

DOI:10.1007/s11426-017-9175-2

Reference yield: 68.0%

Nitrosobenzene (586-96-9) + 2'-Aminobenzanilid (721-47-1) → 2- benzoylaminoazobenzene (7310-83-0)

Guidance literature:

With acetic acid; In ethanol; at 25 ℃; for 15h;

DOI:10.1021/tx0000724

Reference yield:

benzoyl chloride (98-88-4) → 2- benzoylaminoazobenzene (7310-83-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 97 percent / pyridine / 15 h / 25 °C

2: 80 percent / H₂ / 5 percent Pd/C / methanol / 15 h

3: 68 percent / AcOH / ethanol / 15 h / 25 °C

With pyridine; hydrogen; acetic acid; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1021/tx0000724

upstream raw materials:

ethanol

acetic acid

Nitrosobenzene

2'-Aminobenzanilid

Downstream raw materials:

2-aminoazobenzene

2'-Aminobenzanilid

1-(N-acetyl-N-phenylamino)benzimidazole

2-Phenyl-azo-N-methylanilin