4-Pentenamide, 2-[(diphenylmethylene)amino]-

Base Information

Chemical Name:4-Pentenamide, 2-[(diphenylmethylene)amino]-
CAS No.:752233-61-7
Molecular Formula:C18H18N2O
Molecular Weight:278.354
Hs Code.:
DSSTox Substance ID:DTXSID60439711
Nikkaji Number:J2.429.811F

Synonyms:752233-61-7;4-Pentenamide, 2-[(diphenylmethylene)amino]-;DTXSID60439711;2-(Diphenylmethyleneamino)-4-penteneamide

Suppliers and Price of 4-Pentenamide, 2-[(diphenylmethylene)amino]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Pentenamide, 2-[(diphenylmethylene)amino]-

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:278.141913202
Heavy Atom Count:21
Complexity:357

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCC(C(=O)N)N=C(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of 4-Pentenamide, 2-[(diphenylmethylene)amino]-

There total 5 articles about 4-Pentenamide, 2-[(diphenylmethylene)amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: N-benzhydryl-glyoxylic acid imine amide

: 106-95-6
allyl bromide

: 752233-61-7
(+/-)-2-[(diphenylmethylene)amino]-4-pentenamide

Guidance literature:: With potassium tert-butylate; In dichloromethane; at 20 ℃; for 3.5h;

Reference yield: 75.0%

: 79289-52-4
2-[(diphenylmethylene)amino]acetamide

: 106-95-6
allyl bromide

: 752233-61-7
(+/-)-2-[(diphenylmethylene)amino]-4-pentenamide

Guidance literature:: 2-[(diphenylmethylene)amino]acetamide; With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; water; for 0.05h;

allyl bromide; In dichloromethane; water; at 20 ℃;
DOI:10.1139/V06-088

Reference yield:

: 173201-94-0
methyl N-(diphenylmethyl)iminoacetate

: 752233-61-7
(+/-)-2-[(diphenylmethylene)amino]-4-pentenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / NH₃ / methanol / 0.5 h / 20 °C

2: aq. NaOH; Bu₄NHSO₄ / CH₂Cl₂ / 20 °C

With sodium hydroxide; ammonia; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2006.08.096