D-Alanine, N-(2-ethyl-6-methylphenyl)-, methyl ester

Base Information

Chemical Name:D-Alanine, N-(2-ethyl-6-methylphenyl)-, methyl ester
CAS No.:75386-37-7
Molecular Formula:C₁₃H₁₉NO₂
Molecular Weight:221.299
Hs Code.:

Synonyms:(R)-2-(2-Ethyl-6-methyl-phenylamino)-propionic acid methyl ester;(R)-N-(2-ethyl-6-methylphenyl)alanine methyl ester;

Suppliers and Price of D-Alanine, N-(2-ethyl-6-methylphenyl)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-Alanine, N-(2-ethyl-6-methylphenyl)-, methyl ester

Chemical Property:

Boiling Point:141 - 142 °C (12.001 mmHg)
PSA：38.33000
LogP:2.60380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-Alanine, N-(2-ethyl-6-methylphenyl)-, methyl ester

There total 7 articles about D-Alanine, N-(2-ethyl-6-methylphenyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.2%

: 5445-17-0
Methyl 2-bromopropionate

: 24549-06-2
6-ethyl-o-toluidine

: 69516-03-6,75386-37-7,57836-79-0
N-(1'-methoxy-carbonyl-ethyl)-2-methyl-6-ethyl-aniline

Guidance literature:: With sodium hydrogencarbonate; at 120 - 125 ℃; for 19h;
DOI:10.1139/V06-129

Reference yield:

: 69516-03-6,75386-37-7,57836-79-0
N-(1'-methoxy-carbonyl-ethyl)-2-methyl-6-ethyl-aniline

: 82508-03-0
(S)-(-)-N-(2-Ethyl-6-methyl-phenyl)-alanin

: 75386-37-7
(R)-(+)-N-(2-Ethyl-6-methyl-phenyl)-alaninmethylester

Guidance literature:: With Candida antarctica lipase B; sodium hydroxide; phosphate buffer; In diethyl ether; water; at 25 ℃; pH=8.0;
DOI:10.1139/V06-129

Reference yield:

: 24549-06-2
6-ethyl-o-toluidine

: 75386-37-7
(R)-(+)-N-(2-Ethyl-6-methyl-phenyl)-alaninmethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 67.2 percent / NaHCO₃ / 19 h / 120 - 125 °C

2: Candida antarctica lipase B; phosphate buffer; NaOH / H₂O; diethyl ether / 25 °C / pH 8.0

With Candida antarctica lipase B; sodium hydroxide; phosphate buffer; sodium hydrogencarbonate; In diethyl ether; water;
DOI:10.1139/V06-129