Diethyl (3-methylbut-3-en-2-yl)propanedioate

Base Information

Chemical Name:Diethyl (3-methylbut-3-en-2-yl)propanedioate
CAS No.:759-30-8
Molecular Formula:C12H20O4
Molecular Weight:228.288
Hs Code.:
DSSTox Substance ID:DTXSID30553615

Synonyms:759-30-8;Diethyl (3-methylbut-3-en-2-yl)propanedioate;DTXSID30553615

Suppliers and Price of Diethyl (3-methylbut-3-en-2-yl)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Diethyl (3-methylbut-3-en-2-yl)propanedioate

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:228.13615911
Heavy Atom Count:16
Complexity:252

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C(C)C(=C)C)C(=O)OCC

Technology Process of Diethyl (3-methylbut-3-en-2-yl)propanedioate

There total 12 articles about Diethyl (3-methylbut-3-en-2-yl)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40426-44-6
3-methoxy-3-methyl-1-butene

: 105-53-3
diethyl malonate

: 22539-80-6
diethyl (3-methylbut-2-enyl)malonate

: 758-66-7
diethyl 2-(2-methylbut-3-en-2-yl)malonate

: 759-30-8
(dimethyl-1,2 propene-2 yl) propane dioate d'ethyle

Guidance literature:: With sodium hydride; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; In tetrahydrofuran; at 65 ℃; for 36h; Yield given. Yields of byproduct given;
DOI:10.1016/0022-328X(88)80540-0

Reference yield:

: 115-18-4
2-methyl-3-buten-2-ol

: 105-53-3
diethyl malonate

: 22539-80-6
diethyl (3-methylbut-2-enyl)malonate

: 759-30-8
(dimethyl-1,2 propene-2 yl) propane dioate d'ethyle

: 57813-20-4
(E)-(methyl-2 butene-2 yl) propane dioate d'ethyle

: (Z)-(methyl-2 butene-2 yl) propane dioate d'ethyle

Guidance literature:: With sodium hydride; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; In tetrahydrofuran; at 65 ℃; for 36h; Yield given. Further byproducts given. Yields of byproduct given;
DOI:10.1016/0022-328X(88)80540-0

Reference yield:

: 50340-56-2
ethoxy-3 methyl-3 butene-1

: 105-53-3
diethyl malonate

: 22539-80-6
diethyl (3-methylbut-2-enyl)malonate

: 758-66-7
diethyl 2-(2-methylbut-3-en-2-yl)malonate

: 759-30-8
(dimethyl-1,2 propene-2 yl) propane dioate d'ethyle

: 57813-20-4
(E)-(methyl-2 butene-2 yl) propane dioate d'ethyle

Guidance literature:: With sodium hydride; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; In tetrahydrofuran; at 65 ℃; for 36h; Yield given. Further byproducts given. Yields of byproduct given;
DOI:10.1016/0022-328X(88)80540-0