Benzoic acid, 4,4'-[6,11-bis[2,3-dimethoxy-4-(methoxycarbonyl)benzoyl]-1,16-dioxo-2, 6,11,15-tetraazahexadecane-1,16-diyl]bis[2,3-dimethoxy-, dimethyl ester

Base Information

• Chemical Name: Benzoic acid, 4,4'-[6,11-bis[2,3-dimethoxy-4-(methoxycarbonyl)benzoyl]-1,16-dioxo-2, 6,11,15-tetraazahexadecane-1,16-diyl]bis[2,3-dimethoxy-, dimethyl ester
• CAS No.: 75956-65-9
• Molecular Formula: C54H66N4O20
• Molecular Weight: 1091.13

Synonyms:

Chemical Property of Benzoic acid, 4,4'-[6,11-bis[2,3-dimethoxy-4-(methoxycarbonyl)benzoyl]-1,16-dioxo-2, 6,11,15-tetraazahexadecane-1,16-diyl]bis[2,3-dimethoxy-, dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4,4'-[6,11-bis[2,3-dimethoxy-4-(methoxycarbonyl)benzoyl]-1,16-dioxo-2, 6,11,15-tetraazahexadecane-1,16-diyl]bis[2,3-dimethoxy-, dimethyl ester

There total 2 articles about Benzoic acid, 4,4'-[6,11-bis[2,3-dimethoxy-4-(methoxycarbonyl)benzoyl]-1,16-dioxo-2, 6,11,15-tetraazahexadecane-1,16-diyl]bis[2,3-dimethoxy-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Spermine (71-44-3) + 2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid (75956-64-8) → N,N',N'',N'''-tetrakis<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10,14-tetraazatetradecane (75956-65-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; Yield given; Ambient temperature;

DOI:10.1021/jm00134a015

Reference yield:

sodium methyl 2,3-dimethoxyterephthalate (75956-63-7) → N,N',N'',N'''-tetrakis<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10,14-tetraazatetradecane (75956-65-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / SOCl₂

2: NEt₃ / tetrahydrofuran / Ambient temperature

With thionyl chloride; triethylamine; In tetrahydrofuran;

DOI:10.1021/jm00134a015

Reference yield: 67.0%

N,N',N'',N'''-tetrakis<2,3-dimethoxy-4-(carbomethoxy)benzoyl>-1,5,10,14-tetraazatetradecane (75956-65-9) → N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane (75956-67-1)

Guidance literature:

With boron tribromide; In tetrachloromethane; dichloromethane; Ambient temperature;

DOI:10.1021/jm00134a015

upstream raw materials:

Spermine

2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid

sodium methyl 2,3-dimethoxyterephthalate

Downstream raw materials:

N,N',N'',N'''-tetrakis(2,3-dihydroxy-4-carboxybenzoyl)-1,5,10,14-tetraazatetradecane

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 75956-65-9 Benzoic acid, 4,4'-[6,11-bis[2,3-dimethoxy-4-(methoxycarbonyl)benzoyl]-1,16-dioxo-2, 6,11,15-tetraazahexadecane-1,16-diyl]bis[2,3-dimethoxy-, dimethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send