2-(3,3-Dimethylbicyclo[2.2.1]hept-2-yl)acetamide

Base Information

• Chemical Name: 2-(3,3-Dimethylbicyclo[2.2.1]hept-2-yl)acetamide
• CAS No.: 6629-38-5
• Molecular Formula: C11H19NO
• Molecular Weight: 181.2747
• NSC Number: 58151
• DSSTox Substance ID: DTXSID60288928

Synonyms:6629-38-5;2-(3,3-dimethylbicyclo[2.2.1]hept-2-yl)acetamide;NSC58151;3-Camphenilaneacetamide;DTXSID60288928;NSC-58151;Bicyclo[2.2.1]heptane-2-acetamide,3-dimethyl-

Chemical Property of 2-(3,3-Dimethylbicyclo[2.2.1]hept-2-yl)acetamide

Chemical Property:

• Vapor Pressure: 0.000279mmHg at 25°C
• Boiling Point: 322.5°Cat760mmHg
• Flash Point: 148.8°C
• Density: 0.996g/cm³
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 181.146664230
• Heavy Atom Count: 13
• Complexity: 234

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1(C2CCC(C2)C1CC(=O)N)C

Technology Process of 2-(3,3-Dimethylbicyclo[2.2.1]hept-2-yl)acetamide

There total 3 articles about 2-(3,3-Dimethylbicyclo[2.2.1]hept-2-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3,3-dimethyl-[2]norbornyliden)-acetic acid (6008-44-2,22485-80-9) → 3,3-Dimethyl-2-norbornanessigsaeureamid (6629-38-5)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pt / acetic acid / 760 Torr / Ambient temperature

2: SOCl₂ / Heating

3: aq. NH₃

With ammonium hydroxide; thionyl chloride; hydrogen; platinum; In acetic acid;

Reference yield:

3,3-Dimethyl-2-norbornanessigsaeurechlorid (52480-38-3) → 3,3-Dimethyl-2-norbornanessigsaeureamid (6629-38-5)

Guidance literature:

With ammonium hydroxide;

Reference yield:

(3,3-dimethyl-[2]norbornyl)-acetic acid (39850-65-2) → 3,3-Dimethyl-2-norbornanessigsaeureamid (6629-38-5)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / Heating

2: aq. NH₃

With ammonium hydroxide; thionyl chloride;

upstream raw materials:

3,3-Dimethyl-2-norbornanessigsaeurechlorid

(3,3-dimethyl-[2]norbornyl)-acetic acid

(3,3-dimethyl-[2]norbornyliden)-acetic acid

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