Sulfamide, N,N'-bis(1-methyl-1-phenylethyl)-

Base Information

Chemical Name:Sulfamide, N,N'-bis(1-methyl-1-phenylethyl)-
CAS No.:76613-18-8
Molecular Formula:C18H24N2O2S
Molecular Weight:332.467
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Sulfamide, N,N'-bis(1-methyl-1-phenylethyl)-

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Technology Process of Sulfamide, N,N'-bis(1-methyl-1-phenylethyl)-

There total 3 articles about Sulfamide, N,N'-bis(1-methyl-1-phenylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 585-32-0
2-phenyl-2-propylamine

: 76613-18-8
N,N'-bis(1-methyl-1-phenylethyl)sulfamide

Guidance literature:: With sulfuryl dichloride; triethylamine; In dichloromethane; at -78 - 20 ℃; for 23h;
DOI:10.1002/chem.200700820

Reference yield:

: 32366-26-0
cumyl azide

: 76613-18-8
N,N'-bis(1-methyl-1-phenylethyl)sulfamide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / lithium aluminum hydride / diethyl ether / 1.) 12 h, 2.) reflux, 1 h

2: 60 percent / triethylamine, sulfuryl chloride / CH₂Cl₂ / 4 h / -10 °C

With lithium aluminium tetrahydride; sulfuryl dichloride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jo00323a021

Reference yield:

: 617-94-7
1-methyl-1-phenylethyl alcohol

: 76613-18-8
N,N'-bis(1-methyl-1-phenylethyl)sulfamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide, 57percent aq. H₂SO₄ / CHCl₃ / 48 h / ice-bath

2: 68 percent / lithium aluminum hydride / diethyl ether / 1.) 12 h, 2.) reflux, 1 h

3: 60 percent / triethylamine, sulfuryl chloride / CH₂Cl₂ / 4 h / -10 °C

With lithium aluminium tetrahydride; sodium azide; sulfuryl dichloride; sulfuric acid; triethylamine; In diethyl ether; dichloromethane; chloroform;
DOI:10.1021/jo00323a021