[(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene

Base Information

Chemical Name:[(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene
CAS No.:76794-69-9
Molecular Formula:C18H22
Molecular Weight:238.373
Hs Code.:
DSSTox Substance ID:DTXSID20532151
Nikkaji Number:J1.327.870I

Synonyms:76794-69-9;[(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene;DTXSID20532151;2-(4-tert-butyl-1-cyclohexenyl)-ethynyl-benzene;[(4-tert-butyl-1-cyclohexen-1-yl)ethynyl]benzene

Suppliers and Price of [(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:238.172150702
Heavy Atom Count:18
Complexity:360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C1CCC(=CC1)C#CC2=CC=CC=C2

Technology Process of [(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene

There total 6 articles about [(4-tert-Butylcyclohex-1-en-1-yl)ethynyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 77412-96-5
1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene

: 536-74-3
phenylacetylene

: 76794-69-9
1-(2-phenylethynyl)-4-tert-butyl-1-cyclohexene

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

With indium(III) chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane; for 0.5h; Further stages.; Heating;
DOI:10.1021/ol990939t

Reference yield: 95.0%

: 77412-96-5
1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene

: 250643-76-6
tris((2-phenyl)ethynyl)indium

: 76794-69-9
1-(2-phenylethynyl)-4-tert-butyl-1-cyclohexene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 0.5h; Heating;
DOI:10.1021/ja004195m

Reference yield: 86.0%

: 77412-96-5
1-trifluoromethanesulfonyloxy-4-t-butylcyclohexene

: 637-44-5
phenylpropyolic acid

: 76794-69-9
1-(2-phenylethynyl)-4-tert-butyl-1-cyclohexene

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium chloride; silver(l) oxide; In N,N-dimethyl-formamide; at 70 ℃; for 2h; Inert atmosphere;
DOI:10.1002/adsc.200900502