2-(methylthio)-3-Thiophenecarboxaldehyde

Base Information

Chemical Name:2-(methylthio)-3-Thiophenecarboxaldehyde
CAS No.:76834-95-2
Molecular Formula:C6H6OS2
Molecular Weight:158.24100
Hs Code.:2934999090
Mol file:76834-95-2.mol

Synonyms:2-methylthiothiophene-3-carboxaldehyde;2-(METHYLTHIO)THIOPHENE-3-CARBOXALDEHYDE;2-Methylmercapto-thiophenaldehyd-(3);

Suppliers and Price of 2-(methylthio)-3-Thiophenecarboxaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-methylsulfanylthiophene-3-carbaldehyde
500mg
$ 45.00

AOBChem
2-(Methylthio)thiophene-3-carboxaldehyde 97%
500mg
$ 230.00

Total 4 raw suppliers

Chemical Property of 2-(methylthio)-3-Thiophenecarboxaldehyde

Chemical Property:

PSA：70.61000
LogP:2.28250

Purity/Quality:

99% ^*data from raw suppliers

2-methylsulfanylthiophene-3-carbaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(methylthio)-3-Thiophenecarboxaldehyde

There total 2 articles about 2-(methylthio)-3-Thiophenecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872-31-1
3-Bromothiophene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 74-88-4
methyl iodide

: 76834-95-2
2-methylsulfanyl-thiophene-3-carbaldehyde

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, -80 deg C; 2.) ether;

Reference yield:

: 76834-95-2
2-methylsulfanyl-thiophene-3-carbaldehyde

Guidance literature:: 3-Brom-2-methylmercapto-thiophen, 1) Butyllithium in Ae. <-70grad>, 2) N,N-Dimethylformamid 3) wss. HCl;

Reference yield: 74.0%

: 76834-95-2
2-methylsulfanyl-thiophene-3-carbaldehyde

: 1038779-13-3
(4-bromo-2-ethynylphenyl)carbamic acid 1,1-dimethylethyl ester

: tert-butyl (E)-(4-bromo-2-(3-(2-(methylthio)thiophen-3-yl)-3-oxoprop-1-en-1-yl)phenyl)carbamate

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis(dicyclohexylphosphino)methane; In acetone; at 55 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b00390