Ethyl-2-fluoro-5-iodobenzoate

Base Information

• Chemical Name: Ethyl-2-fluoro-5-iodobenzoate
• CAS No.: 773136-66-6
• Molecular Formula: C9H8FIO2
• Molecular Weight: 294.064
• Hs Code.: 2916399090
• Mol file: 773136-66-6.mol

Synonyms:ethyl 2-fluoro-4-methoxybenzoate;ethyl 2-fluoro-5-iodobenzoate;

Chemical Property of Ethyl-2-fluoro-5-iodobenzoate

Chemical Property:

• Vapor Pressure: 0.000721mmHg at 25°C
• Boiling Point: 307.5oC at 760 mmHg
• Flash Point: 139.8oC
• PSA: 26.30000
• Density: 1.728g/cm3
• LogP: 2.60700
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

Ethyl2-Fluoro-5-iodobenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl-2-fluoro-5-iodobenzoate

There total 2 articles about Ethyl-2-fluoro-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.9%

ethanol (64-17-5) + 2-fluoro-5-iodobenzoic acid (124700-41-0) → ethyl 2-fluoro-5-iodobenzoate (773136-66-6)

Guidance literature:

With sulfuric acid; at 100 ℃; for 5h;

Reference yield:

→ ethyl 2-fluoro-5-iodobenzoate (773136-66-6)

Guidance literature:

With sulfuric acid; Reflux;

Reference yield: 7.75%

1-ethenyl-2-pyrrolidinone (88-12-0) + ethyl 2-fluoro-5-iodobenzoate (773136-66-6) → 5-(2-fluoro-5-iodophenyl)-3,4-dihydro-2H-pyrrole

Guidance literature:

1-ethenyl-2-pyrrolidinone; ethyl 2-fluoro-5-iodobenzoate; With sodium hydride; In tetrahydrofuran; water; at 80 ℃; for 3h;

With hydrogenchloride; In tetrahydrofuran; water; at 100 ℃; for 10h;

upstream raw materials:

ethanol

2-fluoro-5-iodobenzoic acid

Downstream raw materials:

C₁₃H₁₅FO₃

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