Phosphorodichloridic acid, 4-chloro-3-methylphenyl ester

Base Information

• Chemical Name: Phosphorodichloridic acid, 4-chloro-3-methylphenyl ester
• CAS No.: 775-13-3
• Molecular Formula: C7H6Cl3O2P
• Molecular Weight: 259.456
• DSSTox Substance ID: DTXSID601199179
• Mol file: 775-13-3.mol

Synonyms:775-13-3;Phosphorodichloridic acid, 4-chloro-3-methylphenyl ester;DTXSID601199179

Chemical Property of Phosphorodichloridic acid, 4-chloro-3-methylphenyl ester

Chemical Property:

• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 257.917100
• Heavy Atom Count: 13
• Complexity: 218

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)OP(=O)(Cl)Cl)Cl

Technology Process of Phosphorodichloridic acid, 4-chloro-3-methylphenyl ester

There total 3 articles about Phosphorodichloridic acid, 4-chloro-3-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chloro-3-methylphenol (59-50-7) → 4-chloro-3-methylphenyl dichlorophosphate (775-13-3)

Guidance literature:

With aluminium trichloride; trichlorophosphate;

DOI:10.1021/ja01536a052

Reference yield:

4-Chloro-3-methylphenol (59-50-7) → 4-chloro-3-methylphenyl dichlorophosphate (775-13-3) + chlorophosphoric acid bis-(4-chloro-3-methyl-phenyl ester) (109311-53-7)

Guidance literature:

With aluminium trichloride; trichlorophosphate; Erhitzen auf Siedetemperatur;

Reference yield:

→ 4-chloro-3-methylphenyl dichlorophosphate (775-13-3)

Guidance literature:

p-Chloro-m-kresol, POCl3;

upstream raw materials:

4-Chloro-3-methylphenol

Downstream raw materials:

2-(4-chloro-3-methyl-phenoxy)-5-nitro-2,3-dihydro-1H-benzo[1,3,2]diazaphosphole 2-oxide

2-(4-chloro-3-methyl-phenoxy)-1,2,3,4-tetrahydro-benzo[1,3,2]diazaphosphinine 2-oxide

2-(4-chloro-3-methyl-phenoxy)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaphosphinine 2-oxide

7-(4-Chloro-3-methyl-phenoxy)-2,3-dimethyl-5,9-dihydro-6,8-dithia-7-phospha-benzocycloheptene 7-oxide