Diethyl [1-(4-nitrophenyl)ethyl]propanedioate

Base Information

Chemical Name:Diethyl [1-(4-nitrophenyl)ethyl]propanedioate
CAS No.:37556-09-5
Molecular Formula:C15H19NO6
Molecular Weight:309.319
Hs Code.:
NSC Number:197106
DSSTox Substance ID:DTXSID40307949

Synonyms:37556-09-5;NSC197106;DTXSID40307949;NSC-197106;diethyl [1-(4-nitrophenyl)ethyl]propanedioate

Suppliers and Price of Diethyl [1-(4-nitrophenyl)ethyl]propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Diethyl [1-(4-nitrophenyl)ethyl]propanedioate

Chemical Property:

Vapor Pressure:8.59E-07mmHg at 25°C
Boiling Point:405.7°Cat760mmHg
Flash Point:155.1°C
Density:1.2g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:309.12123733
Heavy Atom Count:22
Complexity:379

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C(C)C1=CC=C(C=C1)[N+](=O)[O-])C(=O)OCC

Technology Process of Diethyl [1-(4-nitrophenyl)ethyl]propanedioate

There total 7 articles about Diethyl [1-(4-nitrophenyl)ethyl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 14618-12-3
diethyl (1-phenylethyl)malonate

: 37556-09-5
(1-p-Nitro-phenylethyl)-malonsaeurediethylester

Guidance literature:: With sulfuric acid; potassium nitrate; at -10 ℃; for 2h;
DOI:10.1021/jm00034a005

Reference yield:

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 37556-09-5
(1-p-Nitro-phenylethyl)-malonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtONa / 1.) EtOH, 0 deg C, 15 min, 2.) EtOH, 40 deg C, overnight

2: 84 percent / conc. H₂SO₄, KNO₃ / 2 h / -10 °C

With sulfuric acid; sodium ethanolate; potassium nitrate;
DOI:10.1021/jm00034a005

Reference yield:

: 105-53-3
diethyl malonate

: 37556-09-5
(1-p-Nitro-phenylethyl)-malonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtONa / 1.) EtOH, 0 deg C, 15 min, 2.) EtOH, 40 deg C, overnight

2: 84 percent / conc. H₂SO₄, KNO₃ / 2 h / -10 °C

With sulfuric acid; sodium ethanolate; potassium nitrate;
DOI:10.1021/jm00034a005