2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane

Base Information

Chemical Name:2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane
CAS No.:78605-28-4
Molecular Formula:C13H23NSi2
Molecular Weight:249.503
Hs Code.:
DSSTox Substance ID:DTXSID401162493

Synonyms:DTXSID401162493;2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane;78605-28-4

Suppliers and Price of 2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:249.13690281
Heavy Atom Count:16
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)N2[Si](CC[Si]2(C)C)(C)C

Technology Process of 2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane

There total 5 articles about 2,2,5,5-Tetramethyl-1-(3-methylphenyl)-1-aza-2,5-disilacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 91166-50-6
1,1'-(1,2-ethanediyl)bis

: 108-44-1
1-amino-3-methylbenzene

: 78605-28-4
2,2,5,5-Tetramethyl-1-m-tolyl-[1,2,5]azadisilolidine

Guidance literature:: With zinc(II) iodide; for 5h; 1.) 70 deg C, 1 h; 2.) 140 deg C, 4 h;
DOI:10.1016/S0040-4039(01)80126-X

Reference yield: 79.0%

: 13528-93-3
1,2-bis-(chlorodimethylsilyl)ethane

: 108-44-1
1-amino-3-methylbenzene

: 78605-28-4
2,2,5,5-Tetramethyl-1-m-tolyl-[1,2,5]azadisilolidine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -40 ℃;
DOI:10.1016/S0040-4039(01)90439-3

Reference yield:

: 13528-93-3
1,2-bis-(chlorodimethylsilyl)ethane

: 78605-28-4
2,2,5,5-Tetramethyl-1-m-tolyl-[1,2,5]azadisilolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / diethyl ether / 5 h / 0 °C

2: 92 percent / zinc iodide / 5 h / 1.) 70 deg C, 1 h; 2.) 140 deg C, 4 h

With zinc(II) iodide; In diethyl ether;
DOI:10.1016/S0040-4039(01)80126-X