2-Azetidinone, 3-[(1R)-1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-4-[(phenylmethyl)sel eno]-, (3S,4R)-

Base Information

Chemical Name:2-Azetidinone, 3-[(1R)-1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-4-[(phenylmethyl)sel eno]-, (3S,4R)-
CAS No.:786709-79-3
Molecular Formula:C18H29NO2SeSi
Molecular Weight:398.479
Hs Code.:

Synonyms:

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Chemical Property of 2-Azetidinone, 3-[(1R)-1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-4-[(phenylmethyl)sel eno]-, (3S,4R)-

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Technology Process of 2-Azetidinone, 3-[(1R)-1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-4-[(phenylmethyl)sel eno]-, (3S,4R)-

There total 1 articles about 2-Azetidinone, 3-[(1R)-1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-4-[(phenylmethyl)sel eno]-, (3S,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1482-82-2
dibenzyl diselenide

: 76899-07-5,78963-47-0,78963-48-1,78963-60-7,80951-41-3,81275-02-7,85647-75-2,85954-95-6,92217-74-8,104527-11-9,76855-69-1
(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one

: 786709-79-3
(3S,4R)-3-[(R)-tert-butyldimethylsilyloxyethyl]-4-[(phenylmethyl)seleno]-2-azetidinone

Guidance literature:: dibenzyl diselenide; With sodium tetrahydroborate; In ethanol;

(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one; In ethanol; for 1h;
DOI:10.1039/b409242b

Reference yield: 96.0%

: 40400-13-3
2-Iodobenzyl bromide

: 786709-79-3
(3S,4R)-3-[(R)-tert-butyldimethylsilyloxyethyl]-4-[(phenylmethyl)seleno]-2-azetidinone

: 786709-89-5
(3S,4R)-3-[(R)-tert-butyldimethylsilyloxyethyl]-1-[(2-iodophenyl)methyl]-4-[(phenylmethyl)seleno]-2-azetidinone

Guidance literature:: (3S,4R)-3-[(R)-tert-butyldimethylsilyloxyethyl]-4-[(phenylmethyl)seleno]-2-azetidinone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.25h;

2-Iodobenzyl bromide; In tetrahydrofuran; for 4h;
DOI:10.1039/b409242b

Reference yield: 94.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 786709-79-3
(3S,4R)-3-[(R)-tert-butyldimethylsilyloxyethyl]-4-[(phenylmethyl)seleno]-2-azetidinone

: 786709-80-6
tert-butyl 3-[(3S,4R)-(R)-tert-butyldimethylsilyloxyethyl]-2-oxo-4-[(phenylmethyl)seleno]-1-azetidineacetate

Guidance literature:: (3S,4R)-3-[(R)-tert-butyldimethylsilyloxyethyl]-4-[(phenylmethyl)seleno]-2-azetidinone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.166667h;

bromoacetic acid tert-butyl ester; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1039/b409242b