Ethyl 3-((diethoxyphosphoryl)methyl)benzoate

Base Information

Chemical Name:Ethyl 3-((diethoxyphosphoryl)methyl)benzoate
CAS No.:79026-14-5
Molecular Formula:C14H21O5P
Molecular Weight:300.292
Hs Code.:
DSSTox Substance ID:DTXSID40439037
Wikidata:Q82254909

Synonyms:ETHYL 3-((DIETHOXYPHOSPHORYL)METHYL)BENZOATE;79026-14-5;SCHEMBL9454035;DTXSID40439037

Suppliers and Price of Ethyl 3-((diethoxyphosphoryl)methyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethyl 3-((diethoxyphosphoryl)methyl)benzoate

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:300.11266076
Heavy Atom Count:20
Complexity:335

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C1=CC=CC(=C1)CP(=O)(OCC)OCC

Technology Process of Ethyl 3-((diethoxyphosphoryl)methyl)benzoate

There total 5 articles about Ethyl 3-((diethoxyphosphoryl)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 62290-17-9
ethyl 3-bromomethylbenzoate

: 122-52-1
triethyl phosphite

: 79026-14-5
diethyl (3-carbethoxybenzyl)phosphonate

Guidance literature:: for 1h; Heating;
DOI:10.1021/jm00377a022

Reference yield:

: 120-33-2
ethyl 3-methylbenzoate

: 79026-14-5
diethyl (3-carbethoxybenzyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide / azobis(isobutyronitrile) / CCl₄ / 2 h / Heating; irradiation

2: 17.3 g / 4 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane;

Reference yield:

: 1711-06-4
3-Methylbenzoyl chloride

: 79026-14-5
diethyl (3-carbethoxybenzyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 51.5 g / 3 h / Heating

2: N-bromosuccinimide / azobis(isobutyronitrile) / CCl₄ / 2 h / Heating; irradiation

3: 17.3 g / 4 h / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane;