Imidodiphosphorous acid, phenyl-, tetrakis(2-methoxyphenyl) ester

Base Information

• Chemical Name: Imidodiphosphorous acid, phenyl-, tetrakis(2-methoxyphenyl) ester
• CAS No.: 791070-36-5
• Molecular Formula: C34H33NO8P2
• Molecular Weight: 645.585
• Mol file: 791070-36-5.mol

Synonyms:

Chemical Property of Imidodiphosphorous acid, phenyl-, tetrakis(2-methoxyphenyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Imidodiphosphorous acid, phenyl-, tetrakis(2-methoxyphenyl) ester

There total 1 articles about Imidodiphosphorous acid, phenyl-, tetrakis(2-methoxyphenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N,N'-bis(dichlorophosphino)aniline (39652-40-9) + 2-methoxy-phenol (90-05-1) → PhN(P(OC6H4OMe-o)2)2 (791070-36-5)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 24h;

DOI:10.1016/j.jorganchem.2004.08.003

Reference yield: 95.0%

dichloro( 1,5-cyclooctadiene)platinum(ll) (12080-32-9) + PhN(P(OC6H4OMe-o)2)2 (791070-36-5) → [PtCl2(PhN(P(OC6H4OMe-o)2)2)]

Guidance literature:

In acetonitrile; (N2 or Ar); a soln. of ligand added dropwise to a soln. of Pt complex, stirred at room temp. for 3-4 h; concd., petroleum ether added, crystd. at 0°C; elem. anal.;

DOI:10.1016/j.jorganchem.2004.08.003

Reference yield: 94.0%

4,4'-bipyridine (553-26-4) + silver perchlorate + PhN(P(OC6H4OMe-o)2)2 (791070-36-5) → [Ag2(4,4'-bipyridine)(μ-ClO4)[μ-PhN(P(OC6H4OMe-o)2)2]2(ClO4)]n

Guidance literature:

In dichloromethane; (under anaerobic conditions, Schlenk); soln. of 4,4'-bipyridine added dropwise to mixt. of ligand and AgClO4 in CH2Cl2, stirred; filtered, washed with Et2O; elem. anal.;

DOI:10.1021/ic702133f

upstream raw materials:

N,N'-bis(dichlorophosphino)aniline

2-methoxy-phenol

Downstream raw materials:

cis-[Mo(CO)4(PhN(P(OC6H4OMe-o)2)2-κP,κP)]

Cu4(μ2-Cl)2(μ3-Cl)2(PhN(P(OC6H4OMe-o)2)2)2

Cu2(μ2-I)2(NCCH3)2(PhN(P(OC6H4OMe-o)2)2)*CH3CN

[Rh(μ2-Cl)(PhN(P(OC6H4OMe-o)2)2)]2