2,5-Cyclohexadien-1-one, 4-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]cyclohexylmethylene]-2,6- bis(1,1-dimethylethyl)-

Base Information

• Chemical Name: 2,5-Cyclohexadien-1-one, 4-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]cyclohexylmethylene]-2,6- bis(1,1-dimethylethyl)-
• CAS No.: 79320-50-6
• Molecular Formula: C₃₅H₅₂O₂
• Molecular Weight: 504.797
• Mol file: 79320-50-6.mol

Synonyms:

Chemical Property of 2,5-Cyclohexadien-1-one, 4-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]cyclohexylmethylene]-2,6- bis(1,1-dimethylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-Cyclohexadien-1-one, 4-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]cyclohexylmethylene]-2,6- bis(1,1-dimethylethyl)-

There total 2 articles about 2,5-Cyclohexadien-1-one, 4-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]cyclohexylmethylene]-2,6- bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl cyclohexylcarboxylate (4630-82-4) → <(3,5-di-tert-butyl-4-hydroxyphenyl)(3,5-di-tert-butyl-4-oxocyclohexa-2,5-dienylidene)methyl>cyclohexane (79320-50-6)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine

2: 1.) n-butyllithium, (N,N,N',N'-tetramethyldiamino)ethane, 2.) hydrochloric acid / 1.) hexane

With hydrogenchloride; n-butyllithium; N,N,N',N'-tetramethyl-diaminoethane; triethylamine;

DOI:10.1021/ja00411a002

Reference yield:

(4-Bromo-2,6-di-tert-butylphenoxy)trimethylsilane (27329-74-4) + trimethylsilyl cyclohexanecarboxylate (69435-89-8) → <(3,5-di-tert-butyl-4-hydroxyphenyl)(3,5-di-tert-butyl-4-oxocyclohexa-2,5-dienylidene)methyl>cyclohexane (79320-50-6)

Guidance literature:

With hydrogenchloride; n-butyllithium; N,N,N',N'-tetramethyl-diaminoethane; Yield given. Multistep reaction; 1.) hexane;

DOI:10.1021/ja00411a002

Reference yield:

<(3,5-di-tert-butyl-4-hydroxyphenyl)(3,5-di-tert-butyl-4-oxocyclohexa-2,5-dienylidene)methyl>cyclohexane (79320-50-6) → C35H51O2 (79320-55-1)

Guidance literature:

With lead dioxide;

DOI:10.1021/ja00411a002

upstream raw materials:

(4-Bromo-2,6-di-tert-butylphenoxy)trimethylsilane

trimethylsilyl cyclohexanecarboxylate

methyl cyclohexylcarboxylate

Downstream raw materials:

C₃₅H₅₁O₂