Cyclohexene, 1-(bromomethyl)-4-methoxy-3,3-dimethyl-

Base Information

Chemical Name:Cyclohexene, 1-(bromomethyl)-4-methoxy-3,3-dimethyl-
CAS No.:79693-53-1
Molecular Formula:C10H17BrO
Molecular Weight:233.148
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexene, 1-(bromomethyl)-4-methoxy-3,3-dimethyl-

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Technology Process of Cyclohexene, 1-(bromomethyl)-4-methoxy-3,3-dimethyl-

There total 5 articles about Cyclohexene, 1-(bromomethyl)-4-methoxy-3,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 73739-63-6
hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

: 79693-53-1
bromomethyl-1 methoxy-4 dimethyl-3,3 cyclohexene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In acetonitrile; for 3h; Heating;

Reference yield:

: 4454-05-1
2-methoxy-3,4-dihydro-2H-pyran

: 79693-53-1
bromomethyl-1 methoxy-4 dimethyl-3,3 cyclohexene

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating

2: 61 percent / boron trifluoride etherate / Ambient temperature

3: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

4: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

5: 84 percent / carbon tetrabromide, triphenylphosphine / acetonitrile / 3 h / Heating

With sodium tetrahydroborate; carbon tetrabromide; boron trifluoride diethyl etherate; sodium acetate; boron trifluoride methanol complex; triphenylphosphine; In methanol; water; acetic acid; acetonitrile;

Reference yield:

: 4454-02-8
1,1,5,5-tetramethoxy-pentane

: 79693-53-1
bromomethyl-1 methoxy-4 dimethyl-3,3 cyclohexene

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / boron trifluoride etherate / Ambient temperature

2: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

3: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

4: 84 percent / carbon tetrabromide, triphenylphosphine / acetonitrile / 3 h / Heating

With sodium tetrahydroborate; carbon tetrabromide; boron trifluoride diethyl etherate; sodium acetate; triphenylphosphine; In methanol; water; acetic acid; acetonitrile;