AKOS BBS-00007062

Base Information

• Chemical Name: AKOS BBS-00007062
• CAS No.: 80585-40-6
• Molecular Formula: C8H8Cl2O6S2
• Molecular Weight: 335.186
• Mol file: 80585-40-6.mol

Synonyms:4,6-dimethoxy-benzene-1,3-disulfonyl chloride;4,6-dimethoxy-1,3-benzenedisulfonyl chloride;2,4-dimethoxybenzene-1,5-disulfonyl chloride;4,6-Dimethoxy-benzol-1,3-disulfonylchlorid;4,6-dimethoxybenzene-1,3-disulphonyl chloride;4,6-dimethoxybenzene-1,3-disulfonyl dichloride;1,3-Benzenedisulfonyl dichloride,4,6-dimethoxy;

Chemical Property of AKOS BBS-00007062

Chemical Property:

• Boiling Point: 485.3±45.0 °C(Predicted)
• PSA: 103.50000
• Density: 1.590±0.06 g/cm3(Predicted)
• LogP: 3.72040

Purity/Quality:

99% ^*data from raw suppliers

4,6-Dimethoxy-1,3-benzenedisulfonyl dichloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BBS-00007062

There total 4 articles about AKOS BBS-00007062 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4,6-dimethoxybenzene-1,3-disulphonic acid (96519-30-1) → 4,6-dimethoxybenzene-1,3-bis(sulfonyl) chloride (80585-40-6)

Guidance literature:

With phosphorus pentachloride; In pyridine; at 60 ℃; for 4h;

DOI:10.1016/S0040-4039(01)81865-7

Reference yield: 98.0%

dipyridinium 4,6-dimethoxybenzene-1,3-disulphonate (103655-62-5) → 4,6-dimethoxybenzene-1,3-bis(sulfonyl) chloride (80585-40-6)

Guidance literature:

With phosphorus pentachloride; at 60 ℃; for 4h;

DOI:10.1016/S0040-4020(01)96778-X

Reference yield:

1,3-Dimethoxybenzene (151-10-0) → 4,6-dimethoxybenzene-1,3-bis(sulfonyl) chloride (80585-40-6)

Guidance literature:

With chlorosulfonic acid;

DOI:10.1039/j39690001341

upstream raw materials:

4,6-dimethoxybenzene-1,3-disulphonic acid

dipyridinium 4,6-dimethoxybenzene-1,3-disulphonate

1,3-Dimethoxybenzene

Downstream raw materials:

1,3-Dimethoxybenzene

2.4-Dimethoxy-1.5-bis-hydrazinosulfonyl-benzol

4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

Refernces

• 1、 Sekine, Mitsuo,Matsuzaki, Jun-ichi,Hata, Tsujiaki. "PHOSPHOTRIESTER APPROACH TO OLIGOTHYMIDYLATE SYNTHESIS UTILIZING A SIMPLE THYMIDINE UNIT AND A NEW TYPE OF CONDENSING AGENT". . p. 3209 - 3212. Retrieved 2007/10/02.