4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

Base Information

Chemical Name:4,6-dimethoxybenzene-1,3-disulphonyl tetrazole
CAS No.:80596-00-5
Molecular Formula:C₁₀H₁₀N₈O₆S₂
Molecular Weight:402.371
Hs Code.:

Synonyms:4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

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Chemical Property of 4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

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Technology Process of 4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

There total 4 articles about 4,6-dimethoxybenzene-1,3-disulphonyl tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 288-94-8
1H-tetrazole

: 80585-40-6
4,6-dimethoxybenzene-1,3-bis(sulfonyl) chloride

: 80596-00-5
4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

Guidance literature:: With triethylamine; In 1,4-dioxane; dichloromethane; 1.) -5 deg C, 10 min, 2.) RT, 3h;
DOI:10.1016/S0040-4020(01)96778-X

Reference yield:

: 96519-30-1
4,6-dimethoxybenzene-1,3-disulphonic acid

: 80596-00-5
4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 1 h / Ambient temperature

2: 98 percent / PCl₅ / 4 h / 60 °C

3: 75 percent / Et₃N / dioxane; CH₂Cl₂ / 1.) -5 deg C, 10 min, 2.) RT, 3h

With phosphorus pentachloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0040-4020(01)96778-X

Reference yield:

: 103655-62-5
dipyridinium 4,6-dimethoxybenzene-1,3-disulphonate

: 80596-00-5
4,6-dimethoxybenzene-1,3-disulphonyl tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / PCl₅ / 4 h / 60 °C

2: 75 percent / Et₃N / dioxane; CH₂Cl₂ / 1.) -5 deg C, 10 min, 2.) RT, 3h

With phosphorus pentachloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0040-4020(01)96778-X