Cyclohexanaminium, N-(methoxycarbonyl)-N-methylene-

Base Information

Chemical Name:Cyclohexanaminium, N-(methoxycarbonyl)-N-methylene-
CAS No.:807331-78-8
Molecular Formula:C9H16NO2
Molecular Weight:170.232
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanaminium, N-(methoxycarbonyl)-N-methylene-

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Technology Process of Cyclohexanaminium, N-(methoxycarbonyl)-N-methylene-

There total 2 articles about Cyclohexanaminium, N-(methoxycarbonyl)-N-methylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119407-12-4
cyclohexyl(trimethylsilylmethyl)carbamic acid methyl ester

: 807331-78-8
C₉H₁₆NO₂⁽¹⁺⁾

Guidance literature:: With trifluorormethanesulfonic acid; tetrabutylammonium tetrafluoroborate; In dichloromethane; at -78 ℃; Electrolysis; anodic oxidation;
DOI:10.1021/ja0527424

Reference yield:

: 5817-68-5
cyclohexyl-carbamic acid methyl ester

: 807331-78-8
C₉H₁₆NO₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 2 h / 60 °C

1.2: 79 percent / dimethylformamide / 1.5 h / 60 °C

2.1: Bu₄NBF₄; trifluoromethanesulfonic acid / CH₂Cl₂ / -78 °C / Electrolysis; anodic oxidation

With trifluorormethanesulfonic acid; tetrabutylammonium tetrafluoroborate; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0527424

Reference yield: 80.0%

: 31469-15-5
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

: 104173-34-4
2-t-butyl-3-methoxycarbonyl-2,3-dihydrooxazole

: 807331-78-8
C₉H₁₆NO₂⁽¹⁺⁾

: 2-tert-butyl-5-[(cyclohexyl-methoxycarbonyl-amino)-methyl]-3-methoxycarbonyl-4-(1-methoxycarbonyl-1-methylethyl)-oxazolidine

Guidance literature:: 2-t-butyl-3-methoxycarbonyl-2,3-dihydrooxazole; C₉H₁₆NO₂⁽¹⁺⁾; In dichloromethane; at -78 ℃; for 0.0166667h; Inert atmosphere;

1-methoxy-2-methyl-1-trimethylsiloxy-1-propene; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

With triethylamine; at 20 ℃;
DOI:10.1246/cl.2010.404