12-Oxa-2,6,10-triazatetradecanoic acid, 6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-, 1,1-dimethylethyl ester

Base Information

Chemical Name:12-Oxa-2,6,10-triazatetradecanoic acid, 6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-, 1,1-dimethylethyl ester
CAS No.:807381-82-4
Molecular Formula:C45H73N9O6Si
Molecular Weight:864.217
Hs Code.:

12-Oxa-2,6,10-triazatetradecanoic acid,
6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl
silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-,
1,1-dimethylethyl ester

Synonyms:

Suppliers and Price of 12-Oxa-2,6,10-triazatetradecanoic acid, 6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-, 1,1-dimethylethyl ester

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Chemical Property of 12-Oxa-2,6,10-triazatetradecanoic acid, 6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-, 1,1-dimethylethyl ester

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Technology Process of 12-Oxa-2,6,10-triazatetradecanoic acid, 6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-, 1,1-dimethylethyl ester

There total 5 articles about 12-Oxa-2,6,10-triazatetradecanoic acid, 6-[4-[4-(aminomethyl)-1-piperidinyl]-6-[[2-[2-[[(1,1-dimethylethyl)diphenyl silyl]oxy]ethoxy]ethyl]amino]-1,3,5-triazin-2-yl]-13,13-dimethyl-11-oxo-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 7144-05-0
4-Aminomethylpiperidine

: 807381-47-1
{3-[(3-tert-butoxycarbonylamino-propyl)-(4-{2-[2-(tert-butyl-diphenyl-silanyloxy)-ethoxy]-ethylamino}-6-chloro-[1,3,5]triazin-2-yl)-amino]-propyl}-carbamic acid tert-butyl ester

: 807381-82-4
{3-[(4-(4-aminomethyl-piperidin-1-yl)-6-{2-[2-(tert-butyl-diphenyl-silanyloxy)-ethoxy]-ethylamino}-[1,3,5]triazin-2-yl)-(3-tert-butoxycarbonylamino-propyl)-amino]-propyl}-carbamic acid tert-butyl ester

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 8h;
DOI:10.1002/anie.200460031

Reference yield:

: 56-18-8
bis(3-aminopropyl)amine

: 807381-82-4
{3-[(4-(4-aminomethyl-piperidin-1-yl)-6-{2-[2-(tert-butyl-diphenyl-silanyloxy)-ethoxy]-ethylamino}-[1,3,5]triazin-2-yl)-(3-tert-butoxycarbonylamino-propyl)-amino]-propyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / diisopropylethylamine / tetrahydrofuran / 4 h / cooling

2: diisopropylethylamine / tetrahydrofuran / 1 h / cooling

3: 16.6 g / diisopropylethylamine / tetrahydrofuran; methanol / 18 h

4: 95 percent / imidazole; diisopropylethylamine / tetrahydrofuran / 8 h / 20 °C

5: 96 percent / tetrahydrofuran / 8 h / 20 °C

With 1H-imidazole; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.200460031

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 807381-82-4
{3-[(4-(4-aminomethyl-piperidin-1-yl)-6-{2-[2-(tert-butyl-diphenyl-silanyloxy)-ethoxy]-ethylamino}-[1,3,5]triazin-2-yl)-(3-tert-butoxycarbonylamino-propyl)-amino]-propyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / diisopropylethylamine / tetrahydrofuran / 4 h / cooling

2: diisopropylethylamine / tetrahydrofuran / 1 h / cooling

3: 16.6 g / diisopropylethylamine / tetrahydrofuran; methanol / 18 h

4: 95 percent / imidazole; diisopropylethylamine / tetrahydrofuran / 8 h / 20 °C

5: 96 percent / tetrahydrofuran / 8 h / 20 °C

With 1H-imidazole; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.200460031