Benzenemethanol, 2-hydroxy-, monopotassium salt

Base Information

• Chemical Name: Benzenemethanol, 2-hydroxy-, monopotassium salt
• CAS No.: 81426-06-4
• Molecular Formula: C₇H₇O₂*K
• Molecular Weight: 162.23

Synonyms:

Chemical Property of Benzenemethanol, 2-hydroxy-, monopotassium salt

Chemical Property:

Purity/Quality:

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Technology Process of Benzenemethanol, 2-hydroxy-, monopotassium salt

There total 1 articles about Benzenemethanol, 2-hydroxy-, monopotassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

salicylic alcohol (90-01-7) → potassium 2-(hydroxymethyl)phenolate (81426-06-4)

Guidance literature:

With potassium hydroxide; In d⁽⁴⁾-methanol; water-d2;

DOI:10.1002/mrc.3914

Reference yield: 68.0%

potassium 2-(hydroxymethyl)phenolate (81426-06-4) + Zn(C5H4NCH2)2NCH2C6H2(C4H9)2O(H2O)(1+)*ClO4(1-)=Zn(C5H4NCH2)2NCH2C6H2(C4H9)2O(H2O)ClO4 (344613-69-0) + acetone (67-64-1) → Zn(C5H4NCH2)2NCH2C6H2(C4H9)2OOC6H4CH2OH*(CH3)2CO

Guidance literature:

In methanol; byproducts: KClO4; soln. of ligand in MeOH was added to soln. of Zn-complex in MeOH, stirred for 1 h; filtered off, evapd. to dryness, residue was picked up in acetone, exposed to Et2O for 4 d; elem. anal.;

DOI:10.1021/ic001204j

upstream raw materials:

salicylic alcohol

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