1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine

Base Information

Chemical Name:1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine
CAS No.:81815-24-9
Molecular Formula:C20H32ClN3
Molecular Weight:349.947
Hs Code.:
DSSTox Substance ID:DTXSID70510383

Synonyms:81815-24-9;1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine;DTXSID70510383

Suppliers and Price of 1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine

Chemical Property:

XLogP3:7.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:11
Exact Mass:349.2284757
Heavy Atom Count:24
Complexity:321

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCN(CC1)N=NC2=CC=C(C=C2)CCCCCCCCCCl

Technology Process of 1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine

There total 2 articles about 1-{(E)-[4-(9-Chlorononyl)phenyl]diazenyl}piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81815-23-8
1-chloro-9-(p-nitrosophenyl)nonane

: 81815-24-9
1-<4-(9-chlorononyl)phenyl>-3,3-(1,5-pentanediyl)triazene

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaBH₄ / 10percent Pd/C / methanol / 0.5 h / Ambient temperature

2: 1.) NaNO₂, 0.5 N HCl / 1.) 0-5 deg C, 5 min, 2.) 0-5 deg C, 30 min

With hydrogenchloride; sodium tetrahydroborate; sodium nitrite; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00136a040

Reference yield:

: 110-89-4
piperidine

: 81830-39-9
1-chloro-9-(p-aminophenyl)nonane

: 81815-24-9
1-<4-(9-chlorononyl)phenyl>-3,3-(1,5-pentanediyl)triazene

Guidance literature:: With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.) 0-5 deg C, 5 min, 2.) 0-5 deg C, 30 min;
DOI:10.1021/jo00136a040