Stannane, (1-methylheptyl)triphenyl-, (R)-

Base Information

Chemical Name:Stannane, (1-methylheptyl)triphenyl-, (R)-
CAS No.:82823-89-0
Molecular Formula:C26H32Sn
Molecular Weight:463.25
Hs Code.:

Synonyms:

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Chemical Property of Stannane, (1-methylheptyl)triphenyl-, (R)-

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Technology Process of Stannane, (1-methylheptyl)triphenyl-, (R)-

There total 3 articles about Stannane, (1-methylheptyl)triphenyl-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 639-58-7
triphenyltin chloride

: 82823-89-0
Sn(C₆H₅)3(CH₃CHCH₂CH₂CH₂CH₂CH₂CH₃)

Guidance literature:: With lithium; In tetrahydrofuran; under N2, soln. of Ph3SnCl in THF added to Li at 25°C, allowed to stir for 1 h, filtered, soln. of C8H17Br in THF added over 0.5 h, allowed to stir at 25°C for 1 h before adding water; org. layer dried (MgSO4), concd.; GLPC anal.;
DOI:10.1021/ja00374a022

Reference yield:

: 1191-24-8
(S)-(+)-2-bromooctane

: 4167-90-2
lithium triphenylstannide

: 82823-89-0
Sn(C₆H₅)3(CH₃CHCH₂CH₂CH₂CH₂CH₂CH₃)

Guidance literature:: In tetrahydrofuran; at 25°C; enantiomeric excess 100 %;
DOI:10.1021/ja00408a060

Reference yield:

: 4167-90-2
triphenylstannyllithium

: 16844-08-9
(S)-(+)-2-chlorooctane

: 82823-89-0
Sn(C₆H₅)3(CH₃CHCH₂CH₂CH₂CH₂CH₂CH₃)

Guidance literature:: In tetrahydrofuran; THF soln. of (C6H5)3SnLi under N2 filtered through fritted-glass filterinto reaction flask contg. THF soln. of org. compd. for 2 h, mixture stirred for 3 h at 25°C, H2O added;