N-METHYL-N-4-PIPERIDINYLACETAMIDE

Base Information

• Chemical Name: N-METHYL-N-4-PIPERIDINYLACETAMIDE
• CAS No.: 83180-55-6
• Molecular Formula: C8H16N2O
• Molecular Weight: 156.22500
• Hs Code.: 2933399090
• Mol file: 83180-55-6.mol

Synonyms:4-(N-methyl-N-acetylamino)piperidine;4-(N-methylacetamido)piperidine;4-(N-acetyl-N-methylamino)piperidine;N-Methyl-N-(4-piperidyl)acetamide;N-Methyl-N-piperidin-4-yl-acetamide;

Chemical Property of N-METHYL-N-4-PIPERIDINYLACETAMIDE

Chemical Property:

• PSA: 32.34000
• LogP: 0.54550

Purity/Quality:

97% ^*data from raw suppliers

N-Methyl-N-(piperidin-4-yl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-METHYL-N-4-PIPERIDINYLACETAMIDE

There total 2 articles about N-METHYL-N-4-PIPERIDINYLACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

→ 4-(N-acetyl-N-methylamino)-piperidine (83180-55-6)

Guidance literature:

Reference yield:

4-(acetyl-methyl-amino)-piperidine-1-carboxylic acid tert-butyl ester (197727-57-4) → 4-(N-acetyl-N-methylamino)-piperidine (83180-55-6)

Guidance literature:

With hydrogenchloride; In water; ethyl acetate; at 20 ℃; for 16h;

Reference yield: 95.0%

4-(N-acetyl-N-methylamino)-piperidine (83180-55-6) + 4-bromo-2-(3,4-dichlorophenyl)-2-methylbutyric acid methyl ester (1093078-84-2) → 4-[4-(acetyl(methylamino))piperidin-1-yl]-2-(3,4-dichlorophenyl)-2-methylbutyric acid methyl ester (1131739-62-2)

Guidance literature:

In N,N-dimethyl acetamide; at 55 ℃; for 86h;

DOI:10.1021/jm900948q

upstream raw materials:

4-(acetyl-methyl-amino)-piperidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

4-[4-(acetyl(methylamino))piperidin-1-yl]-2-(3,4-dichlorophenyl)-2-methylbutyric acid methyl ester

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