3-Butynoic acid, 2,2-dimethyl-4-phenyl-, ethyl ester

Base Information

Chemical Name:3-Butynoic acid, 2,2-dimethyl-4-phenyl-, ethyl ester
CAS No.:83188-31-2
Molecular Formula:C14H16O2
Molecular Weight:216.28
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Butynoic acid, 2,2-dimethyl-4-phenyl-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of 3-Butynoic acid, 2,2-dimethyl-4-phenyl-, ethyl ester

There total 2 articles about 3-Butynoic acid, 2,2-dimethyl-4-phenyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1483-82-5
phenylethynyl chloride

: 97-62-1
Ethyl isobutyrate

: 83188-31-2
ethyl 2,2-dimethyl-4-phenyl-3-butynoate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/chem.201303795

Reference yield:

: 600-00-0
ethyl 2-bromoisobutyrate

: 536-74-3
phenylacetylene

: 83188-31-2
ethyl 2,2-dimethyl-4-phenyl-3-butynoate

Guidance literature:: With Sodium thiosulfate pentahydrate; tetra-(n-butyl)ammonium iodide; sodium carbonate; In water; at 65 ℃; for 2.5h; Inert atmosphere; UV-irradiation;
DOI:10.1002/chem.201600219