Technology Process of Bis[bis(trimethylsilyl)methyl]phosphane
There total 1 articles about Bis[bis(trimethylsilyl)methyl]phosphane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
benzene-d6;
dissolution in benzene; free phosphine is present in 3% to total phosphorus content at 21°C and ca. 20% at 80°C, shift of the equil. upon addn. of 1 equiv of phosphine ligand or (RhCl(COD))2 confirmes the reversibility of the reaction; (31)P and (1)H NMR spectral data;