4,1-Benzoxazepin-2(3H)-one, 7-chloro-5-(2,3-dimethoxyphenyl)-1,5-dihydro-1-(3-hydroxy-2,2-dimethyl propyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-, (3R,5S)-

Base Information

• Chemical Name: 4,1-Benzoxazepin-2(3H)-one, 7-chloro-5-(2,3-dimethoxyphenyl)-1,5-dihydro-1-(3-hydroxy-2,2-dimethyl propyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-, (3R,5S)-
• CAS No.: 839724-93-5
• Molecular Formula: C30H32ClNO7
• Molecular Weight: 554.04

Synonyms:

Chemical Property of 4,1-Benzoxazepin-2(3H)-one, 7-chloro-5-(2,3-dimethoxyphenyl)-1,5-dihydro-1-(3-hydroxy-2,2-dimethyl propyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-, (3R,5S)-

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 4,1-Benzoxazepin-2(3H)-one, 7-chloro-5-(2,3-dimethoxyphenyl)-1,5-dihydro-1-(3-hydroxy-2,2-dimethyl propyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-, (3R,5S)-

There total 1 articles about 4,1-Benzoxazepin-2(3H)-one, 7-chloro-5-(2,3-dimethoxyphenyl)-1,5-dihydro-1-(3-hydroxy-2,2-dimethyl propyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-, (3R,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (3R,5S)-7-chloro-5-(2,3-dimethoxyphenyl)-1-(3-hydroxy-2,2-dimethylpropyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-1,5-dihydro-4,1-benzoxazepin-2(3H)-one (839724-93-5)

Guidance literature:

Reference yield:

(3R,5S)-7-chloro-5-(2,3-dimethoxyphenyl)-1-(3-hydroxy-2,2-dimethylpropyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-1,5-dihydro-4,1-benzoxazepin-2(3H)-one (839724-93-5) + ethyl bromoacetate (105-36-2) → (4-{[(3R,5S)-7-chloro-5-(2,3-dimethoxyphenyl)-1-(3-hydroxy-2,2-dimethylpropyl)-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepin-3-yl]acetyl}phenoxy)acetic acid

Guidance literature:

(3R,5S)-7-chloro-5-(2,3-dimethoxyphenyl)-1-(3-hydroxy-2,2-dimethylpropyl)-3-[2-(4-hydroxyphenyl)-2-oxoethyl]-1,5-dihydro-4,1-benzoxazepin-2(3H)-one; ethyl bromoacetate; With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 30 ℃; for 2h;

With sodium hydroxide; ethanol; water; In tetrahydrofuran; at 20 - 30 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; ethanol; water;

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