4,1-Benzoxazepine-3-butanethioamide, 1-[2-(acetyloxy)-2-methylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,2,3, 5-tetrahydro-2-oxo-, (3R,5S)-

Base Information

• Chemical Name: 4,1-Benzoxazepine-3-butanethioamide, 1-[2-(acetyloxy)-2-methylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,2,3, 5-tetrahydro-2-oxo-, (3R,5S)-
• CAS No.: 839725-11-0
• Molecular Formula: C27H33ClN2O6S
• Molecular Weight: 549.088

Synonyms:

Chemical Property of 4,1-Benzoxazepine-3-butanethioamide, 1-[2-(acetyloxy)-2-methylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,2,3, 5-tetrahydro-2-oxo-, (3R,5S)-

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Technology Process of 4,1-Benzoxazepine-3-butanethioamide, 1-[2-(acetyloxy)-2-methylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,2,3, 5-tetrahydro-2-oxo-, (3R,5S)-

There total 1 articles about 4,1-Benzoxazepine-3-butanethioamide, 1-[2-(acetyloxy)-2-methylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,2,3, 5-tetrahydro-2-oxo-, (3R,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-[(3R,5S)-7-chloro-3-(3-cyanopropyl)-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate (839725-10-9) → 2-[(3R,5S)-3-(4-amino-4-thioxobutyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-1,1-dimethylethyl acetate (839725-11-0)

Guidance literature:

With hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate; In water; ethyl acetate;

Reference yield:

2-[(3R,5S)-3-(4-amino-4-thioxobutyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-1,1-dimethylethyl acetate (839725-11-0) + ethyl (2-chloroaceto)acetate (638-07-3) → C34H41ClN2O8S

Guidance literature:

In ethanol; at 90 ℃; for 2h;

upstream raw materials:

3-[(3R,5S)-7-chloro-3-(3-cyanopropyl)-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

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