4,1-Benzoxazepine-3-butanenitrile, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-

Base Information

Chemical Name:4,1-Benzoxazepine-3-butanenitrile, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-
CAS No.:839725-10-9
Molecular Formula:C28H33ClN2O6
Molecular Weight:529.033
Hs Code.:

4,1-Benzoxazepine-3-butanenitrile,
1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1,
2,3,5-tetrahydro-2-oxo-, (3R,5S)-

Synonyms:

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Chemical Property of 4,1-Benzoxazepine-3-butanenitrile, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-

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Technology Process of 4,1-Benzoxazepine-3-butanenitrile, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)-

There total 2 articles about 4,1-Benzoxazepine-3-butanenitrile, 1-[3-(acetyloxy)-2,2-dimethylpropyl]-7-chloro-5-(2,3-dimethoxyphenyl)-1, 2,3,5-tetrahydro-2-oxo-, (3R,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 839725-45-0
(2E)-4-[(3R,5S)-1-(3-acetoxy-2,2-dimethylpropyl)-7-chloro-5-(2,3-dimethoxyphenyl)-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepin-3-yl]-2-butenenitrile

: 839725-10-9
3-[(3R,5S)-7-chloro-3-(3-cyanopropyl)-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

Guidance literature:: With methanol; magnesium; for 19h; Product distribution / selectivity;

Reference yield:

: C₂₈H₃₁ClN₂O₆

: 75-36-5
acetyl chloride

: 839725-10-9
3-[(3R,5S)-7-chloro-3-(3-cyanopropyl)-5-(2,3-dimethoxyphenyl)-2-oxo-2,3-dihydro-4,1-benzoxazepin-1(5H)-yl]-2,2-dimethylpropyl acetate

Guidance literature:: C₂₈H₃₁ClN₂O₆; With methanol; magnesium; for 2h;

acetyl chloride; With triethylamine; In dichloromethane; Product distribution / selectivity;