Benzene, 1-methyl-3-(2-propenylthio)-

Base Information

Chemical Name:Benzene, 1-methyl-3-(2-propenylthio)-
CAS No.:77102-55-7
Molecular Formula:C10H12S
Molecular Weight:164.271
Hs Code.:
NSC Number:115078
DSSTox Substance ID:DTXSID60227892
Nikkaji Number:J1.830.073G
Wikidata:Q83107729

Synonyms:Benzene, 1-methyl-3-(2-propenylthio)-;77102-55-7;NSC115078;allyl 3-methylphenyl sulfide;SCHEMBL6057139;DTXSID60227892;NSC 115078;NSC-115078

Suppliers and Price of Benzene, 1-methyl-3-(2-propenylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzene, 1-methyl-3-(2-propenylthio)-

Chemical Property:

Vapor Pressure:0.13mmHg at 25°C
Boiling Point:225.4°Cat760mmHg
Flash Point:88.9°C
Density:0.99g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:164.06597156
Heavy Atom Count:11
Complexity:120

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)SCC=C

Technology Process of Benzene, 1-methyl-3-(2-propenylthio)-

There total 1 articles about Benzene, 1-methyl-3-(2-propenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-40-7
toluene-3-thiol

: 106-95-6
allyl bromide

: 77102-55-7
m-methylphenylallyl thioether

Guidance literature:: With potassium carbonate; In ethanol; at 20 ℃; for 12h;
DOI:10.1039/c6gc02681h

Reference yield: 95.0%

: 77102-55-7
m-methylphenylallyl thioether

: 922-67-8
propynoic acid methyl ester

: methyl (Z)-2-((m-tolylthio)methylene)pent-4-enoate

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]gold bis(trifluoromethanesulfonyl)imidate; In toluene; at 60 ℃; for 10h; stereoselective reaction;
DOI:10.1002/anie.201802540

Reference yield: 89.0%

: (E)-2-diazo-4-phenyl-1-(3,4,5-trimethyl-1H-pyrazol-1-yl)but-3-en-1-one

: 77102-55-7
m-methylphenylallyl thioether

: (E)-2-styryl-2-(m-tolylthio)-1-(3,4,5-trimethyl-1H-pyrazol-1-yl)pent-4-en-1-one

Guidance literature:: With C₃₈H₅₈N₄O₄; nickel dichloride; silver(I) triflimide; In dichloromethane; at 40 ℃; for 0.0833333h; enantioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.7b12486