N-Allyl-2,4-dinitroaniline

Base Information

• Chemical Name: N-Allyl-2,4-dinitroaniline
• CAS No.: 7403-39-6
• Molecular Formula: C9H9N3O4
• Molecular Weight: 223.188
• Mol file: 7403-39-6.mol

Synonyms:2,4-Dinitro-N-allyl-anilin;N-allyl-2,4-dinitro-aniline;Aniline,N-allyl-2,4-dinitro;Benzenamine,4-dinitro-N-2-propenyl;

Chemical Property of N-Allyl-2,4-dinitroaniline

Chemical Property:

• Vapor Pressure: 7.63E-06mmHg at 25°C
• Boiling Point: 375.7°Cat760mmHg
• Flash Point: 181°C
• PSA: 103.67000
• Density: 1.389g/cm³
• LogP: 3.22030

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Allyl-2,4-dinitroaniline

There total 3 articles about N-Allyl-2,4-dinitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + allyl bromide (106-95-6) → allyl-(2,4-dinitrophenyl)amine (7403-39-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.3762/bjoc.11.203

Reference yield: 70.0%

1-chloro-2,4-dinitro-benzene (97-00-7) + 1-amino-2-propene (107-11-9,30551-89-4) → allyl-(2,4-dinitrophenyl)amine (7403-39-6)

Guidance literature:

In ethanol; at 80 ℃; for 24h;

DOI:10.14233/ajchem.2018.20784

Reference yield:

2,4-dinitrobromobenzene (584-48-5) + 1-amino-2-propene (107-11-9,30551-89-4) → allyl-(2,4-dinitrophenyl)amine (7403-39-6)

Guidance literature:

With ethanol;

upstream raw materials:

1-chloro-2,4-dinitro-benzene

1-amino-2-propene

2,4-dinitrobromobenzene

2,4-Dinitrofluorobenzene

Downstream raw materials:

C₉H₁₀FN₃O₄

N-allyl-4-nitrobenzene-1,2-diamine