1,3-Hexanediol, (3R)-

Base Information

Chemical Name:1,3-Hexanediol, (3R)-
CAS No.:84314-30-7
Molecular Formula:C6H14O2
Molecular Weight:118.176
Hs Code.:

Synonyms:

Suppliers and Price of 1,3-Hexanediol, (3R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1,3-Hexanediol, (3R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:

Useful:

Technology Process of 1,3-Hexanediol, (3R)-

There total 1 articles about 1,3-Hexanediol, (3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 92418-71-8
(2R,3R)-2,3-epoxy-1-hexanol

: 84314-30-7
(R)-(-)-hexane-1,3-diol

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; at 0 ℃; for 1h; regioselective reaction;
DOI:10.1016/j.tetlet.2019.150944

Reference yield: 94.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 84314-30-7
(R)-(-)-hexane-1,3-diol

: (4R)-2-(4-methoxyphenyl)-4-propyl-1,3-dioxane

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2019.150944

Reference yield:

: 84314-30-7
(R)-(-)-hexane-1,3-diol

: 458-88-8
coniine

Guidance literature:: Multi-step reaction with 8 steps

1.1: SOCl₂

2.1: RuO₂; NaIO₄

3.1: NaH / N,N-dimethyl-acetamide / 20 °C

3.2: N,N-dimethyl-acetamide / 20 h / 164 °C

4.1: 87 percent / Al/Hg / tetrahydrofuran

5.1: 89 percent / LiAlH₄

6.1: Et₃N

7.1: NaH / dimethylformamide

8.1: RedAl

With ruthenium(IV) oxide; sodium periodate; aluminum amalgam; lithium aluminium tetrahydride; thionyl chloride; sodium hydride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; N,N-dimethyl acetamide; N,N-dimethyl-formamide; 1.1: Cyclization / 2.1: Oxidation / 3.1: Deprotonation / 3.2: Alkylation / 4.1: Reduction / 5.1: Reduction / 6.1: Tosylation / 7.1: Cyclization / 8.1: Reduction;