bromo(N,N-dimethylmethanamine)dihydridoboron

Base Information

Chemical Name:bromo(N,N-dimethylmethanamine)dihydridoboron
CAS No.:5275-42-3
Molecular Formula:C3H11BBrN
Molecular Weight:151.842
Hs Code.:

Synonyms:

Suppliers and Price of bromo(N,N-dimethylmethanamine)dihydridoboron

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of bromo(N,N-dimethylmethanamine)dihydridoboron

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bromo(N,N-dimethylmethanamine)dihydridoboron

There total 2 articles about bromo(N,N-dimethylmethanamine)dihydridoboron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 617-86-7
triethylsilane

: 10294-33-4
boron tribromide

: 121-44-8
triethylamine

: 5275-42-3
(CH₃)3N*BH₂Br

: 1722-26-5
triethylamine-borane

Guidance literature:: nickel; In neat (no solvent); heating;;

Reference yield:

: 75-22-9
trimethylamine-borane

: 10294-33-4
boron tribromide

: 5275-42-3
(CH₃)3N*BH₂Br

: 19287-45-7
diborane

Guidance literature:: In benzene; dropwise addn. of BBr3 in benzene to the benzene-soln. (molar ratio 3:1), boiling for 20min;;
DOI:10.1021/ic50088a026

Reference yield: 52.0%

: 5275-42-3
(CH₃)3N*BH₂Br

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 1135446-19-3
[H₂B(ImMes)2]Br

Guidance literature:: In chlorobenzene; under Ar atm. 1-mesitylimidazole and Me3NBH2Br (2:1) in chlorobenzene were stirred at reflux for 10-15 h; react. mixt. was cooled to room temp., solvent was removed in vacuo, residue was dissolved in CH2Cl2, pptd. with Et2O dried in air and in vacuo and crystd. from CHCl3; elem. anal.;
DOI:10.1021/om8010933