2,4-cyclohexadien-1-one, 2-[[[2-(dimethylamino)ethyl]ethylamino]methyl]-4-methyl-6-[[[3-(methylthio)propyl]amino]methylene]-, compd. with 1,1-ethanediol, nickel nickel(2+) salt, hydrate (2:6:3:2:2)

Base Information

• Chemical Name: 2,4-cyclohexadien-1-one, 2-[[[2-(dimethylamino)ethyl]ethylamino]methyl]-4-methyl-6-[[[3-(methylthio)propyl]amino]methylene]-, compd. with 1,1-ethanediol, nickel nickel(2+) salt, hydrate (2:6:3:2:2)
• CAS No.: 7226-40-6
• Molecular Formula: C₉H₁₆O₅
• Molecular Weight: 204.223

Synonyms:

Chemical Property of 2,4-cyclohexadien-1-one, 2-[[[2-(dimethylamino)ethyl]ethylamino]methyl]-4-methyl-6-[[[3-(methylthio)propyl]amino]methylene]-, compd. with 1,1-ethanediol, nickel nickel(2+) salt, hydrate (2:6:3:2:2)

Chemical Property:

• Vapor Pressure: 3.79E-09mmHg at 25°C
• Boiling Point: 473.9°Cat760mmHg
• Flash Point: 240.4°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-cyclohexadien-1-one, 2-[[[2-(dimethylamino)ethyl]ethylamino]methyl]-4-methyl-6-[[[3-(methylthio)propyl]amino]methylene]-, compd. with 1,1-ethanediol, nickel nickel(2+) salt, hydrate (2:6:3:2:2)

There total 5 articles about 2,4-cyclohexadien-1-one, 2-[[[2-(dimethylamino)ethyl]ethylamino]methyl]-4-methyl-6-[[[3-(methylthio)propyl]amino]methylene]-, compd. with 1,1-ethanediol, nickel nickel(2+) salt, hydrate (2:6:3:2:2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2,3-anhydro-4,6-benzylidene-α-D-allopyranoside (66537-92-6) → methyl 2,3-anhydro-4,6-di-O-methyl-α-D-allopyranoside (7226-40-6)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted aqueous sulfuric acid; methanol

2: silver oxide

With methanol; sulfuric acid; silver(l) oxide;

DOI:10.1002/hlca.19470300517

Reference yield:

methyl 2,3-anhydro-α-D-allopyranoside (3257-61-2) + methyl iodide (74-88-4) → methyl 2,3-anhydro-4,6-di-O-methyl-α-D-allopyranoside (7226-40-6)

Guidance literature:

With silver(l) oxide;

DOI:10.1002/hlca.19470300517 DOI:10.1039/jr9380000472

Reference yield:

→ methyl 2,3-anhydro-4,6-di-O-methyl-α-D-allopyranoside (7226-40-6)

Guidance literature:

With methanol; chloroform; sodium methylate; Behandeln des Reaktionsprodukts mit Methyljodid und Silberoxid;

DOI:10.1039/jr9380001088

upstream raw materials:

methyl 2,3-anhydro-α-D-allopyranoside

methyl iodide

methyl-(2-chloro-2-deoxy-α-D-altropyranoside)

methyl 2,3-anhydro-4,6-benzylidene-α-D-allopyranoside

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