4-Amino-1-methylpyridin-1-ium iodide

Base Information

• Chemical Name: 4-Amino-1-methylpyridin-1-ium iodide
• CAS No.: 7680-59-3
• Molecular Formula: C6H9 N2 . I
• Molecular Weight: 237.06
• Hs Code.: 2933399090
• European Community (EC) Number: 806-872-6
• Mol file: 7680-59-3.mol

Synonyms:4-aminopyridine methiodide;4-APMI

Chemical Property of 4-Amino-1-methylpyridin-1-ium iodide

Chemical Property:

• Vapor Pressure: 0.0165mmHg at 25°C
• Boiling Point: 255.2°C at 760 mmHg
• Flash Point: 131.8°C
• PSA: 39.64000
• LogP: 1.64510
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 235.98105
• Heavy Atom Count: 9
• Complexity: 64.9

Purity/Quality:

4-Amino-1-methylpyridin-1-ium iodide >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=CC=C(C=C1)N.[I-]

Technology Process of 4-Amino-1-methylpyridin-1-ium iodide

There total 1 articles about 4-Amino-1-methylpyridin-1-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-aminopyridine (504-24-5) + methyl iodide (74-88-4) → N-methyl-4-aminopyridinium iodide (7680-59-3)

Guidance literature:

for 8h;

DOI:10.1039/c5tc03499j

Reference yield: 29.0%

(2S,5R)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1]octane-2-carboxylic acid (1174020-25-7,2064219-13-0) + N-methyl-4-aminopyridinium iodide (7680-59-3) → C20H23N4O3(1+)*I(1-)

Guidance literature:

With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In acetonitrile; at 60 ℃; for 1h;

DOI:10.1016/j.bmcl.2013.12.101

Reference yield:

tetrabromobenzoquinone (488-48-2) + N-methyl-4-aminopyridinium iodide (7680-59-3) → 2C6H9N2(1+)*2I(1-)*C6Br4O2

Guidance literature:

In [⁽²⁾H₆]acetone; at 5 ℃;

DOI:10.1039/d1ce01156a

upstream raw materials:

4-aminopyridine

methyl iodide

Downstream raw materials:

C₂₃H₁₉ClN₃O₂⁽¹⁺⁾*I^(1-)