1-Iodo-9,10-anthraquinone

Base Information

• Chemical Name: 1-Iodo-9,10-anthraquinone
• CAS No.: 3485-80-1
• Molecular Formula: C14H7IO2
• Molecular Weight: 334.113
• NSC Number: 338059
• UNII: QGC72BJ8JC
• DSSTox Substance ID: DTXSID90188402
• Nikkaji Number: J450.087C
• Wikidata: Q83060210
• Mol file: 3485-80-1.mol

Synonyms:1-Iodo-9,10-anthraquinone;Anthraquinone, 1-iodo-;9,10-Anthracenedione, 1-iodo-;3485-80-1;NSC-338059;1-iodoanthracene-9,10-dione;1-IODO-9,10-DIHYDROANTHRACENE-9,10-DIONE;iodoanthraquinone;C14H7IO2;1-Iodoanthraquinone;NSC338059;NSC 338059;QGC72BJ8JC;9, 1-iodo-;1-Iodo-9,10-anthracenedione;SCHEMBL10716268;DTXSID90188402;AKOS000528544;EU-0066929;InChI=1/C14H7IO2/c15-11-7-3-6-10-12(11)14(17)9-5-2-1-4-8(9)13(10)16/h1-7

Chemical Property of 1-Iodo-9,10-anthraquinone

Chemical Property:

• Vapor Pressure: 9.72E-09mmHg at 25°C
• Boiling Point: 462.6°Cat760mmHg
• Flash Point: 233.6°C
• Density: 1.844g/cm³
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 333.94908
• Heavy Atom Count: 17
• Complexity: 352

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)C3=C(C2=O)C(=CC=C3)I

Technology Process of 1-Iodo-9,10-anthraquinone

There total 3 articles about 1-Iodo-9,10-anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-(9,10-antraquinone)diazonium nitrate → 1-iodo-9,10-anthraquinone (3485-80-1)

Guidance literature:

With potassium iodide; for 24h;

DOI:10.1002/1521-3765(20020315)8:6<1395::AID-CHEM1395>3.0.CO;2-L

Reference yield: 83.0%

1-amino-9,10-anthracenedione (82-45-1) → 1-iodo-9,10-anthraquinone (3485-80-1)

Guidance literature:

With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In acetonitrile; at 20 ℃; for 1h;

DOI:10.1055/s-2006-958936

Reference yield:

→ 1-iodo-9,10-anthraquinone (3485-80-1)

Guidance literature:

aus Anthrachinon-1-diazoniumsalz und KI;

DOI:10.1246/bcsj.50.2982

upstream raw materials:

1-amino-9,10-anthracenedione

Downstream raw materials:

1-(4-methylphenyl)-9-anthrone

1-(3-isopropylphenyl)-9-anthrone

1-(4-isopropylphenyl)-9-anthrone

1-(4-methylphenyl)-9-[(trifluoromethylsulfonyl)oxy]anthracene