1-(3,5-Dichlorophenyl)ethanaMine

Base Information

Chemical Name:1-(3,5-Dichlorophenyl)ethanaMine
CAS No.:84499-83-2
Molecular Formula:C8H9Cl2N
Molecular Weight:190.072
Hs Code.:
Mol file:84499-83-2.mol

Synonyms:[1-(3,5-dichlorophenyl)ethyl]amine;1-(3,5-Dichlorophenyl)ethanamine;[1-(3,5-dichlorophenyl)-ethyl]-amine;

Suppliers and Price of 1-(3,5-Dichlorophenyl)ethanaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(3,5-Dichlorophenyl)ethanamine
10mg
$ 45.00

SynQuest Laboratories
1-(3,5-Dichlorophenyl)ethylamine
5 g
$ 495.00

SynQuest Laboratories
1-(3,5-Dichlorophenyl)ethylamine
1 g
$ 165.00

SynQuest Laboratories
1-(3,5-Dichlorophenyl)ethylamine
250 mg
$ 61.00

Crysdot
1-(3,5-Dichlorophenyl)ethanamine 95+%
1g
$ 556.00

Chemenu
1-(3,5-Dichlorophenyl)ethanamine 95%
1g
$ 520.00

Alichem
1-(3,5-Dichlorophenyl)ethanamine
1g
$ 528.68

Total 15 raw suppliers

Chemical Property of 1-(3,5-Dichlorophenyl)ethanaMine

Chemical Property:

PSA：26.02000
LogP:3.71340
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

1-(3,5-Dichlorophenyl)ethanamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(3,5-Dichlorophenyl)ethanaMine

There total 6 articles about 1-(3,5-Dichlorophenyl)ethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10203-08-4
3,5-dichlorobenzaldehyde

: 84499-83-2
(+/-)-α-(3,5-dichlorophenyl)ethylamine

Guidance literature:: 3,5-dichlorobenzaldehyde; With lithium hexamethyldisilazane; In tetrahydrofuran; at -30 - -5 ℃; for 1h;

With methyllithium; In tetrahydrofuran; diethyl ether; at -60 - -55 ℃; for 1h;

With hydrogenchloride; sodium hydroxide; water; more than 3 stages;

Reference yield:

: 917-54-4
methyllithium

: 84499-83-2
(+/-)-α-(3,5-dichlorophenyl)ethylamine

Guidance literature:: 3,5-dichlorobenzaldehyde; With lithium hexamethyldisilazane; In tetrahydrofuran; at -30 - -5 ℃; for 1h;

methyllithium; In tetrahydrofuran; diethyl ether; at -60 - -55 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; water; at -60 ℃; pH=2;

Reference yield:

: 51-36-5
3,5-dichlorobenzoic acid

: 84499-83-2
(+/-)-α-(3,5-dichlorophenyl)ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 10.5 g / tetrahydrofuran; diethyl ether / 1.) 0 deg C, 10 min, 2.) 30 min

2: 1.) formic acid, formamide, 2.) 3 N hydrochloric acid / 1.) H₂O, 165-180 deg C, 20 h, 2.) reflux, 48 h

With hydrogenchloride; formic acid; formamide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00344a026