N-(1,3-benzodioxol-5-yl)-3-iodobenzamide

Base Information

Chemical Name:N-(1,3-benzodioxol-5-yl)-3-iodobenzamide
CAS No.:6183-79-5
Molecular Formula:C₃₄H₄₇NO₄
Molecular Weight:533.751
Hs Code.:
DSSTox Substance ID:DTXSID70361115
Wikidata:Q82143258

Synonyms:N-(1,3-benzodioxol-5-yl)-3-iodobenzamide;6183-79-5;CBMicro_002660;Oprea1_147774;Cholecalciferol, p-nitrobenzoate;DTXSID70361115;SMSF0016668;AKOS001391441;CB04274;BIM-0002651.P001;AG-670/15545076;SR-01000230133;SR-01000230133-1;Z27647543;9,10-Secocholesta-5,7,10(19)-trien-3-ol, 4-nitrobenzoate, (3.beta.,5Z,7E)-

Suppliers and Price of N-(1,3-benzodioxol-5-yl)-3-iodobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(1,3-benzodioxol-5-yl)-3-iodobenzamide

Chemical Property:

Vapor Pressure:5.94E-06mmHg at 25°C
Boiling Point:379.2°C at 760 mmHg
Flash Point:183.2°C
Density:1.821g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:366.97054
Heavy Atom Count:19
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C=C2)NC(=O)C3=CC(=CC=C3)I

Technology Process of N-(1,3-benzodioxol-5-yl)-3-iodobenzamide

There total 6 articles about N-(1,3-benzodioxol-5-yl)-3-iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-97-0
vitamin D₃

: 62-23-7
4-nitro-benzoic acid

: 6183-79-5,60413-84-5,60413-85-6,62743-69-5
Epivitamin D₃-p-nitrobenzoat

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene;
DOI:10.1002/hlca.19760590622

Reference yield:

: 67-97-0
vitamin D₃

: 122-04-3
4-nitro-benzoyl chloride

: 6183-79-5,60413-84-5,60413-85-6,62743-69-5
vitamin D3 p-nitrobenzoate

Guidance literature:: With pyridine;
DOI:10.1021/ja01220a033

Reference yield:

: 434-16-2
7-dehydrocholesterol

: 6183-79-5,60413-84-5,60413-85-6,62743-69-5
vitamin D3 p-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / Irradiation_.UV-Licht; unter Luftausschluss; Reinigung ueber das O-<3.5-Dinitro-benzoyl>-Derivat, das O-<3.5-Dinitro-4-methyl-benzoyl>-Derivat oder das Allophanoyl-Derivat

2: pyridine

With pyridine; diethyl ether;