1H-Isoindole-1,3(2H)-dione, 2-[trans-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]cyclohexyl]-

Base Information

Chemical Name:1H-Isoindole-1,3(2H)-dione, 2-[trans-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]cyclohexyl]-
CAS No.:847416-23-3
Molecular Formula:C20H29NO3Si
Molecular Weight:359.541
Hs Code.:

Synonyms:trans-N-(4-tert-butyldimethylsilyloxycyclohexyl)phthalimide;trans-2-(4-(tert-butyl-dimethyl-silyloxy)-cyclohexyl)-isoindole-1,3-dione;

Suppliers and Price of 1H-Isoindole-1,3(2H)-dione, 2-[trans-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]cyclohexyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1H-Isoindole-1,3(2H)-dione, 2-[trans-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]cyclohexyl]-

Chemical Property:

PSA：46.61000
LogP:4.55350

Purity/Quality:: More than 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Isoindole-1,3(2H)-dione, 2-[trans-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]cyclohexyl]-

There total 4 articles about 1H-Isoindole-1,3(2H)-dione, 2-[trans-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]cyclohexyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 99337-98-1
2-((1R,4R)-4-hydroxycyclohexyl) isoindoline-1,3-dione

: 847416-23-3
2-((1R,4R)-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)isoindoline-1,3-dione

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; toluene; at 40 ℃; Cooling with ice;

Reference yield:

: 50910-54-8
trans-4-aminocyclohexanol hydrochloride

: 847416-23-3
2-((1R,4R)-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water / 1 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide; toluene / 40 °C / Cooling with ice

With 1H-imidazole; potassium carbonate; In water; N,N-dimethyl-formamide; toluene;

Reference yield:

: trans-4-hydroxycyclohexylamine hydrochloride

: 847416-23-3
2-((1R,4R)-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water / 3 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 - 40 °C

With 1H-imidazole; potassium carbonate; In water; N,N-dimethyl-formamide;