2-Pyridinecarboxylic acid, 5-[[[(1S)-1-[(1,1-dimethylethoxy)methyl]-2-methoxy-2-oxoethyl]amino]thi oxomethyl]-6-phenyl-, methyl ester

Base Information

Chemical Name:2-Pyridinecarboxylic acid, 5-[[[(1S)-1-[(1,1-dimethylethoxy)methyl]-2-methoxy-2-oxoethyl]amino]thi oxomethyl]-6-phenyl-, methyl ester
CAS No.:847778-83-0
Molecular Formula:C22H26N2O5S
Molecular Weight:430.525
Hs Code.:

Synonyms:

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Chemical Property of 2-Pyridinecarboxylic acid, 5-[[[(1S)-1-[(1,1-dimethylethoxy)methyl]-2-methoxy-2-oxoethyl]amino]thi oxomethyl]-6-phenyl-, methyl ester

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Technology Process of 2-Pyridinecarboxylic acid, 5-[[[(1S)-1-[(1,1-dimethylethoxy)methyl]-2-methoxy-2-oxoethyl]amino]thi oxomethyl]-6-phenyl-, methyl ester

There total 9 articles about 2-Pyridinecarboxylic acid, 5-[[[(1S)-1-[(1,1-dimethylethoxy)methyl]-2-methoxy-2-oxoethyl]amino]thi oxomethyl]-6-phenyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 847778-82-9
5-(2-tert-butoxy-1-methoxycarbonyl-ethylcarbamoyl)-6-phenyl-pyridine-2-carboxylic acid methyl ester

: 847778-83-0
5-(2-tert-butoxy-1-methoxycarbonyl-ethylthiocarbamoyl)-6-phenyl-pyridine-2-carboxylic acid methyl ester

Guidance literature:: With Lawessons reagent; In benzene; for 66h; Heating;
DOI:10.1021/jo048106q

Reference yield:

: 847778-78-3
3-tert-butoxy-2-(3-oxo-3-phenyl-propionylamino)-propionic acid methyl ester

: 847778-83-0
5-(2-tert-butoxy-1-methoxycarbonyl-ethylthiocarbamoyl)-6-phenyl-pyridine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / NH₄OAc; AcOH / toluene / Heating

2: 95 percent / methanol / 60 h / 20 °C

3: 96 percent / Lawesson's reagent / benzene / 66 h / Heating

With Lawessons reagent; ammonium acetate; acetic acid; In methanol; toluene; benzene;
DOI:10.1021/jo048106q

Reference yield:

: 847778-79-4
(S)-2-((Z)-3-Amino-3-phenyl-acryloylamino)-3-tert-butoxy-propionic acid methyl ester

: 847778-83-0
5-(2-tert-butoxy-1-methoxycarbonyl-ethylthiocarbamoyl)-6-phenyl-pyridine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / methanol / 60 h / 20 °C

2: 96 percent / Lawesson's reagent / benzene / 66 h / Heating

With Lawessons reagent; In methanol; benzene;
DOI:10.1021/jo048106q