Carbamic acid, [(1S,2S)-2-[[[4-[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]benzoyl ]amino]phenyl]sulfonyl]amino]-1,2-diphenylethyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S,2S)-2-[[[4-[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]benzoyl ]amino]phenyl]sulfonyl]amino]-1,2-diphenylethyl]-, 1,1-dimethylethyl ester
CAS No.:847908-00-3
Molecular Formula:C74H69N3O11S
Molecular Weight:1208.44
Hs Code.:

Carbamic acid,
[(1S,2S)-2-[[[4-[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]benzoyl
]amino]phenyl]sulfonyl]amino]-1,2-diphenylethyl]-, 1,1-dimethylethyl
ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S,2S)-2-[[[4-[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]benzoyl ]amino]phenyl]sulfonyl]amino]-1,2-diphenylethyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Carbamic acid, [(1S,2S)-2-[[[4-[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]benzoyl ]amino]phenyl]sulfonyl]amino]-1,2-diphenylethyl]-, 1,1-dimethylethyl ester

There total 5 articles about Carbamic acid, [(1S,2S)-2-[[[4-[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]benzoyl ]amino]phenyl]sulfonyl]amino]-1,2-diphenylethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 174877-79-3
3,5-bis(3,5-bis(benzyloxy)benzyloxy)benzoic acid

: 847907-98-6
(S,S)-N-Boc-N'-(4-aminophenylsulfonyl)-1,2-diphenylethylenediamine

: 847908-00-3
((1S,2S)-2-{4-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzoylamino]-benzenesulfonylamino}-1,2-diphenyl-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: With pyridine; triphenyl phosphite; at 95 ℃; for 24h;
DOI:10.1021/jo048317v

Reference yield:

: [(1S,2S)-2-(4-Nitro-benzenesulfonylamino)-1,2-diphenyl-ethyl]-carbamic acid tert-butyl ester

: 847908-00-3
((1S,2S)-2-{4-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzoylamino]-benzenesulfonylamino}-1,2-diphenyl-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂; Pd/C; HCOONH₄

2: (PhO)3P; pyridine

With pyridine; triphenyl phosphite; palladium on activated charcoal; hydrogen; ammonium formate;
DOI:10.1039/b104160f

Reference yield:

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 847908-00-3
((1S,2S)-2-{4-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzoylamino]-benzenesulfonylamino}-1,2-diphenyl-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NEt₃

2: 99 percent / DIPEA

3: 95 percent / H₂; Pd/C; HCOONH₄

4: (PhO)3P; pyridine

With pyridine; triphenyl phosphite; palladium on activated charcoal; hydrogen; ammonium formate; triethylamine; N-ethyl-N,N-diisopropylamine;
DOI:10.1039/b104160f