Phosphorin, 4-(dichloromethylene)-1,4-dihydro-3,5-dimethyl-1-phenyl-

Base Information

Chemical Name:Phosphorin, 4-(dichloromethylene)-1,4-dihydro-3,5-dimethyl-1-phenyl-
CAS No.:848338-07-8
Molecular Formula:C14H13Cl2P
Molecular Weight:283.137
Hs Code.:

Synonyms:

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Chemical Property of Phosphorin, 4-(dichloromethylene)-1,4-dihydro-3,5-dimethyl-1-phenyl-

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Technology Process of Phosphorin, 4-(dichloromethylene)-1,4-dihydro-3,5-dimethyl-1-phenyl-

There total 1 articles about Phosphorin, 4-(dichloromethylene)-1,4-dihydro-3,5-dimethyl-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 130760-07-5
4-(dichloromethylene)-1,4-dihydro-3,5-dimethyl-1-phenylphosphinine 1-oxide

: 848338-07-8
4-dichloromethylene-1,4-dihydrophosphinine

Guidance literature:: With trichlorosilane; In dichloromethane; benzene; at 0 ℃;
DOI:10.1016/j.jorganchem.2004.08.051

Reference yield: 80.0%

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 848338-07-8
4-dichloromethylene-1,4-dihydrophosphinine

: 845291-65-8
(4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride

Guidance literature:: In dichloromethane; under Ar; Rh complex in CH2Cl2 added to soln. of ligand in CH2Cl2 at 25°C over 10-15 min; stirred for 0.5 h; solvent evapd. to dryness; CH2Cl2 added; filtered; pentane added dropwise to filtrate; stored at 26°C overnight; filtered; crystals driedin vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2004.08.051

Reference yield: 73.0%

: 14220-64-5,39958-10-6,15617-18-2
bis(benzonitrile)palladium(II) chloride

: 848338-07-8
4-dichloromethylene-1,4-dihydrophosphinine

: 845291-71-6
PdCl₂(P(C₆H₅)CHC(CH₃)C(CCl₂)C(CH₃)CH)2

Guidance literature:: In benzene; under Ar; Pd complex in benzene added to soln. of ligand in benzene at 0°C over 10 min; stirred for 0.5 h; warmed to room temp.; solvent evapd.; CH2Cl2 added; filtered; pentane added to filtrate; stored at 26°C overnight; filtered; crystals dried in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2004.08.051