(4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride

Base Information

Chemical Name:(4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride
CAS No.:845291-65-8
Molecular Formula:C₂₄H₂₈Cl₄PRh
Molecular Weight:592.178
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Chemical Property of (4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride

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Technology Process of (4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride

There total 1 articles about (4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 848338-07-8
4-dichloromethylene-1,4-dihydrophosphinine

: 845291-65-8
(4-dichloromethylene-1,4-dihydrophosphinine) pentamethylcyclopentadienyl rhodium dichloride

Guidance literature:: In dichloromethane; under Ar; Rh complex in CH2Cl2 added to soln. of ligand in CH2Cl2 at 25°C over 10-15 min; stirred for 0.5 h; solvent evapd. to dryness; CH2Cl2 added; filtered; pentane added dropwise to filtrate; stored at 26°C overnight; filtered; crystals driedin vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2004.08.051