(1,1-Dimethylethyl)phenylphosphinothioic chloride

Base Information

Chemical Name:(1,1-Dimethylethyl)phenylphosphinothioic chloride
CAS No.:62839-84-3
Molecular Formula:C10H14ClPS
Molecular Weight:232.7099
Hs Code.:
NSC Number:201413
Nikkaji Number:J832.047K

Synonyms:62839-84-3;(1,1-Dimethylethyl)phenylphosphinothioic chloride;Phosphinothioic chloride, (1,1-dimethylethyl)phenyl-;MCLWOWVVBCYSMN-UHFFFAOYSA-N;NSC201413;NSC 201413;NSC-201413;tert-Butyl(phenyl)phosphinothioic chloride #;Phosphine sulfide, (chloro)(t-butyl)(phenyl)

Suppliers and Price of (1,1-Dimethylethyl)phenylphosphinothioic chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (1,1-Dimethylethyl)phenylphosphinothioic chloride

Chemical Property:

Vapor Pressure:0.00293mmHg at 25°C
Boiling Point:294°Cat760mmHg
Flash Point:131.6°C
Density:1.15g/cm³
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:232.0242363
Heavy Atom Count:13
Complexity:214

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)P(=S)(C1=CC=CC=C1)Cl

Technology Process of (1,1-Dimethylethyl)phenylphosphinothioic chloride

There total 4 articles about (1,1-Dimethylethyl)phenylphosphinothioic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.4%

: 4923-85-7
tert-butylphenylphosphinic acid chloride

: 62839-84-3
tert.-butyl-phenylthiophosphinic chloride

Guidance literature:: With tetraphosphorus decasulfide; at 160 ℃; for 5h;
DOI:10.1080/10426509608037973

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 62839-84-3
tert.-butyl-phenylthiophosphinic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / AlCl₃

2: 85.4 percent / P₂S₅ / 5 h / 160 °C

With aluminium trichloride; tetraphosphorus decasulfide;
DOI:10.1080/10426509608037973