2-(4-Hydroxyphenyl)glyoxylohydroximoyl chloride

Base Information

• Chemical Name: 2-(4-Hydroxyphenyl)glyoxylohydroximoyl chloride
• CAS No.: 34911-46-1
• Molecular Formula: C8H6 Cl N O3
• Molecular Weight: 199.594
• Hs Code.: 2925290090
• DSSTox Substance ID: DTXSID0041305
• Mol file: 34911-46-1.mol

Synonyms:Benzeneethanimidoyl chloride, N,4-dihydroxy-alpha-oxo-;para-Hydroxy-2-oxo-phenylacethydroxymic acid chloride;SCHEMBL204419;DTXSID0041305;LS-30255;2-(4-Hydroxyphenyl)glyoxylohydroximoyl chloride;Q27282388

Chemical Property of 2-(4-Hydroxyphenyl)glyoxylohydroximoyl chloride

Chemical Property:

• Boiling Point: 425.9°Cat760mmHg
• Flash Point: 211.4°C
• PSA: 69.89000
• Density: 1.43g/cm³
• LogP: 1.60140
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 199.0036207
• Heavy Atom Count: 13
• Complexity: 221

Purity/Quality:

99% ^*data from raw suppliers

N,4-DIHYDROXY-ALPHA-OXOBENZENEACETIMIDOYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=O)C(=NO)Cl)O
• Isomeric SMILES: C1=CC(=CC=C1C(=O)/C(=N/O)/Cl)O

Technology Process of 2-(4-Hydroxyphenyl)glyoxylohydroximoyl chloride

There total 2 articles about 2-(4-Hydroxyphenyl)glyoxylohydroximoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-hydroxyphenacyl chloride (6305-04-0) → (4-hydroxy-phenyl)-glyoxylohydroximoyl chloride (34911-46-1)

Guidance literature:

With diethyl ether; n-Butyl nitrite; Einleiten von Chlorwasserstoff;

DOI:10.1021/jo01199a002

Reference yield:

→ (4-hydroxy-phenyl)-glyoxylohydroximoyl chloride (34911-46-1)

Guidance literature:

entspr. ω-Cl-Acetophenon, Isopropylnitrit;

Reference yield:

1-methyl-4-nitrosobenzene (623-11-0) + (4-hydroxy-phenyl)-glyoxylohydroximoyl chloride (34911-46-1) → 4-hydroxy-benzoic acid (99-96-7)

Guidance literature:

DOI:10.1021/jo01199a002

upstream raw materials:

p-hydroxyphenacyl chloride

Downstream raw materials:

4-hydroxy-benzoic acid