Styrene, alpha-chloro-p-nitro-

Base Information

Chemical Name:Styrene, alpha-chloro-p-nitro-
CAS No.:10140-97-3
Molecular Formula:C8H6 Cl N O2
Molecular Weight:183.60
Hs Code.:2904909090
UNII:777RM62EL5
DSSTox Substance ID:DTXSID10143912
Nikkaji Number:J48.678G
Wikidata:Q83007959
Mol file:10140-97-3.mol

Synonyms:alpha-Chloro-p-nitrostyrene;Styrene, alpha-chloro-p-nitro-;10140-97-3;1-(1-chloroethenyl)-4-nitrobenzene;BRN 2360211;777RM62EL5;Benzene, 1-(1-chloroethenyl)-4-nitro-;0-05-00-00480 (Beilstein Handbook Reference);UNII-777RM62EL5;SCHEMBL8370241;DTXSID10143912;Styrene, .alpha.-chloro-p-nitro-;CHLORO-P-NITROSTYRENE, ALPHA;LS-147212

Suppliers and Price of Styrene, alpha-chloro-p-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Styrene, alpha-chloro-p-nitro-

Chemical Property:

Vapor Pressure:0.0146mmHg at 25°C
Melting Point:63.5°C
Refractive Index:1.5560 (estimate)
Boiling Point:265.9°Cat760mmHg
Flash Point:114.6°C
PSA：45.82000
Density:1.293g/cm³
LogP:3.32750
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:183.0087061
Heavy Atom Count:12
Complexity:192

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C1=CC=C(C=C1)[N+](=O)[O-])Cl

Technology Process of Styrene, alpha-chloro-p-nitro-

There total 6 articles about Styrene, alpha-chloro-p-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 937-31-5
(4-Nitrophenyl)acetylene

: 10140-97-3
1-(1-chloroethenyl)-4-nitrobenzene

Guidance literature:: With hydrogenchloride; chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II); triphenylphosphine; In diethyl ether; 1,2-dichloro-ethane; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201505144

Reference yield: 78.0%

: 100-19-6
(4-nitrophenyl)ethanone

: 10140-97-3
1-(1-chloroethenyl)-4-nitrobenzene

: 76213-14-4
1-(1,1-dichloroethyl)-4-nitrobenzene

Guidance literature:: With tetra-(n-butyl)ammonium iodide; 1,2-dichloro-ethane; triphenylphosphine; at 120 ℃; for 5h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01058

Reference yield:

: 937-31-5
(4-Nitrophenyl)acetylene

: 10140-97-3
1-(1-chloroethenyl)-4-nitrobenzene

: 3756-35-2
1-(2-chlorovinyl)-4-nitrobenzene

Guidance literature:: With C₃₇H₆₁AuClO₂P; HCl·DMPU; In nitromethane; at 20 ℃; Overall yield = 74 %; regioselective reaction;
DOI:10.1021/acscatal.7b02567