Technology Process of Methyl, [6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]dioxyphenyl-
There total 4 articles about Methyl, [6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]dioxyphenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,2-dibromo-1,1,2,2-tetrafluoroethane; oxygen;
In
trichlorofluoromethane;
at -88.15 ℃;
Irradiation;
DOI:10.1002/ejoc.200400437
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Mg turnings; iodine; 1,2-dibromoethane / diethyl ether / 3 h / Heating
1.2: toluene; diethyl ether / Heating
2.1: N2O4; sodium acetate / CCl4 / 1 h / 0 - 5 °C
3.1: LiAlH4 / diethyl ether / 0.5 h / 0 °C
4.1: oxygen; CF2BrCF2Br / CCl3F / -88.15 °C / Irradiation
With
lithium aluminium tetrahydride; 1,2-dibromo-1,1,2,2-tetrafluoroethane; iodine; oxygen; sodium acetate; dinitrogen tetraoxide; magnesium; ethylene dibromide;
In
tetrachloromethane; diethyl ether; trichlorofluoromethane;
DOI:10.1002/ejoc.200400437
- Guidance literature:
-
Multi-step reaction with 2 steps
1: LiAlH4 / diethyl ether / 0.5 h / 0 °C
2: oxygen; CF2BrCF2Br / CCl3F / -88.15 °C / Irradiation
With
lithium aluminium tetrahydride; 1,2-dibromo-1,1,2,2-tetrafluoroethane; oxygen;
In
diethyl ether; trichlorofluoromethane;
DOI:10.1002/ejoc.200400437
